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~VAG~~f CORE LABORATORIES DUAL I T Y C O N T R O L R E S U L T S Job Number.: 982396 Report Date.: 10/19/98 CUSTOMER: Greys [one PROJECT: DTRY 484-03 ATtN: Jeff Spinzig Test Method........: EPA 340.2 Batch .............: 39114 Analyst...: mjf Me [hod Description.: Fluoride (ISE) Units .............: mg/L Pa remeter..........: Fluoride (F) DC Lab ID Reagent CCB CCV G9805198 MS 982382-1 G9805198 MD 982382-1 CCB DC Result QC Result True Value Orig. Value Calc. Result • Limits Date Time 0.0 0.1 09/15/1998 1630 3.0 3.003003 99.9 X 90.110 09/15/1998 1630 1.9 1.000000 1.0 90.0 X 75.125 09/15/1998 1630 0.9 1.0 10.5 R 20 09/15/1998 1630 0.0 0.1 09/15/1998 1630 Test Method........: EPA 353.2 Batch .............: 39096 Analyst...: tlp Method Description.: Nitrogen, N02, N03 (Auto Cd Red.) Units .............; m9/L Parameter..........: Nitrate + Nitrite as N aC Lab 10 Reagent DC Result ICB 0.00 ICL G980506A 1.00 MD 982449-1 2.10 MS 982449-1 G980805A 3.11 CCV G980805A 2.06 CCB 0.00 MD 982394-1 0.27 MS 982394-1 G980805A 1.21 MD 982394-3 0.18 MS 982394-3 G980805A 1.06 LCS C980506A 1.04 CCV G980805A 2.11 CCB 0.00 CCV C980605A 2.04 CCB 0.00 QL Result True Value Ori 9. Value Calc. Result ' Limits Date time 0.05 09/15/1998 0830 1.000000 100.0 X 90.110 09/15/1998 0839 1.98 5.9 R 20 09/15/1998 0913 1.000000 1.98 113.0 X 75-125 09/15/1998 0921 2.000000 103.0 X 90-110 09/15/1998 1039 0.05 09/15/1998 1056 O.Z7 0.0 R 20 09/15/1998 1130 1.000000 0.27 94.0 X 75.125 09/15/1998 1139 0.19 0.01 A 0.05 09/15/1998 1156 1.000000 0.19 87.0 X 75.125 09/15/1998 1204 1.000000 104.0 X 80-120 09/15/1998 1230 2.000000 105.5 X 90-110 09/15/1998 1239 0.05 09/15/1998 1256 2.000000 102.0 X 90.110 09/15/1998 1421 0.05 09/15/1998 1430 Test Method........: EPA 160.1 Batch .............: 39044 Analyst...: mjf Method Description.: Solids, Total Dissolved (TOS) Units .............: mg/L Parameter..........: Solids, Total Dissolved (TDS) OC lab ID Reagent OC Result QC Result True Value Orig. Value Calc. Result ' Limits Dale Time LCS G980817 502 500 100.4 X 80-120 09/10/1998 1820 MD 982396-1 181 183 1.1 R 20 09/10/1998 1820 MB 0 10 09/10/1998 1820 Test Method........: EPA 150.1 Batch .............: 38903 Analyst...: mjf Method Description.: pH Units .............: pH Units Parameter..........: pH DC Lab ID Reagent DC Result DC Result True Value Orig. Value Calc. Result • Limits Date Time CCV 980265 6.98 7.00 99.7 X 90.110 09/09/1998 1105 MD 982384-1 11.95 11.95 0.0 R 20 09/09/1998 1105 CCV 980265 6.98 7.00 99.7 X 90-110 09/09/1998 1105 CCV 980265 7.01 7.00 100.1 X 90.110 09/09/1998 1105 MD 982347-8 8.41 8.42 0.1 R 20 09/09/1998 1105 MD 982347-3 8.59 8.58 0.1 R 20 09/09/1998 1105 Page 6 ` X=X REC, R=RPD, A=ABS Diff., D=X Diff. ., ..