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MATR]% SPIKE SAMPLE SVALIIATION REPORT General Chemistry Client Lot # ._.: D3H080357 Matrix-.._-.._.: WATER Date Sampled .._: 08/13/03 14:55 Date Received..: 08/13/03 - PERC ENT RECOVERY RPD PREPARATION - PREP PARAMETER RECOVERY LIMI TS RPD LIMITS- METHOD ANALYSIS DATE BATCH # Ammonia as N WO#: FVT371CK-MS/FVT371CL-MSD MS Lot-Sample #: D3H070280-001 95 (44 - 130) MCAWW 350.1 08/15/03 3228205 95 (44 - 130) 0.08 (0-30) MCAWW 350.1 ~ - --08/15/03 3228205 Dilution Factor:l - -~- Analysis Time..: 15:00 -' - - Chloride WO#: FWANNICA-MS/FWANNICC-MSD MS Lot-Sample #: D3H140310-009 102 (90 - 110) ~ MCAWW 325.2 08/18/03 3231285 100 (90 -110) 1.7 (0-10) MCAWW 325.2 08/18/03 :- 3231285 Dilution Factor: 1 ' Analysis Time..: 15:00 ' Chloride WO#: FWD2RIAT-MS/FWD2RiAU-MSD MS Lot-Sample #: D3H150330-001 90 (90 - 110) MCAWW 325.2 .08/18/03 3231283 85 N (90 - 110) 1.4 (0-10) MCAWW 325.2 08/18/03 3231283 Dilution Factor: 1 Analysis Time..: 16:00 Fluoride WO#: FVOPGICE-MS/FVOPGICF-MSD MS Lot-Sample #: D3H080357-003 102 (87 - 107) SM18 4500-F C 08/22/03 3234488 100 (87 - 107) 2,5 (0-10) 5M18 4500-F C 08/22/03 3234488 Dilution Factor: 1 Analysis Time..: 16:00 Fluoride WO#: FV3VOICP-MS/FV3VOiCQ-MSD MS Lot-Sample #: 03 H110207-001 107 (87 - 107) SM18 4500-F C 08(22/03 3234487 107 (87 - 107) 0.0 (0-10) SM18 4500-F C 08/22/03 3234487 Dilution Factor: 1 Analysis Time..: 16:00 ~ . Fluoride WO#: FVBA3 ICN-MS/FVBA3ICP-MSD MS Lot-Sample #: D3 H130327-002 107 (87 - 107) - SM18 4500-F C 08/22/03 3234489 106 (87 - 107) 0.83 (0-10) SM18 4500-F C 08f22j03 3234489 Dilution Factor: 1 Anal yeie Time..: 16:00 Nitrate-Nitri te WO#: FVT371CM-MS/FVT371CN-MSD MS Lot-Sample #: D3H070280-001 92 (62 - 119) MCAWW 353.2 08/15/03 3228216 95 (62 - 119) 2.8 (0-30) MCAWW 353.2 08/15/03 3228216 Dilution Factor: 1 Analye is Time..: 15:00 (Continued on next page) 46