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MATRI% SPIKH, SAMPLH DATA RHPORT <br />TOTAL Metals <br />Client Lot #_..: D3H080357 Matrix_..,..,,_: WATER <br />Date Sampled__,: 08/08/03 08:00 Date Received..: 08/08/03 <br />SAMPLE SPIKE MEASRD PERCNT PREPARATION- WORK <br />PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE ORDER # <br /> <br />MS Lot-Sample #: D3H080357-001 Prep Batch #...: 3221191 <br />Aluminum <br />0.20 2.00 2.46 N mg/L 113 MCAWW 200.7 08/12-08/13/03 FVON2ICL <br />0.20 -_ -2:-00-~~ 2.41 N mg/L 110 1.9 MCAWW-200.7 08/12-08/13/03 FVON2ICR <br /> Dilu tion Factor: 1 - <br /> Analysis Time..: 13:04 <br />Beryllium <br />ND <br />ND <br />Cadmium <br />ND <br />ND <br />Calcium <br />450 <br />450 <br />Chromium <br />ND <br />ND <br />Iron <br />1.7 <br />1.7 <br />Magnesium <br />180 <br />18,0. <br />0.0500 0.0452~~mg/L 9C <br />0.0500 0.0454 mg/L 91 <br />Dilution Factor: 1 <br />Analysis Time..: 13:09 <br />0.0500 0.0492 mg/L 98 <br />0.0500 0.0484 mg/L ~97 <br /> Dilution Factor: 1 <br /> Analysis Time. .: 13:09 <br />50.0 484 mg/L <br /> Qualifiers: NC,MSB <br />50.0 486 mg/L <br /> Qualifiers: NC,MSB <br /> Dilution Factor: 1 <br /> Anal yeie Time. .: 13:04 <br />0.200 0.199 mgjL 99 <br />0.200 0.197 mg/L 98 <br />Dilution Factor: 1 <br />Anal yeie Time..: 13:04 <br />1.00 2.64 mg/L 93 <br />1.00 2.65 mgjL 9. <br />Dilution Factor: 1 <br />Analysis Time..: 13:04 <br />50.0 <br />50.0 <br />.` MCAWW.200.7 08/12-08/13/03FVON2ICG <br />0.46, MCAWW 200.7 08/12-08/13/03 FVON21Ck <br />MCAWW 200.7 OS/12-08/13/03 FVON2ICL ~ <br />1.5 MCAWW 200.7 08/12-08/13/03 FVON2ICM <br />MCAWW 200.7 08/12-08/13/03 FVON2ICJ <br />MCAWW 200.7 08/12-08/13/03 FVON2ICK <br />- MCAWW 200.7 08j12-08/13J03 FVON2ICN <br />1.1 MCAWW 200.7 08/12-OB/13/03 FVON2ICP <br />MCAWW 200.7 08/12-08/13/03 FVON2ICQ <br />0.23 MCAWW 200.7 08j12-08/13/03 FVON2ICR <br />228 mg/L 98 MCAWW 200.7 08/12-08/13/03 F'VON2ICV <br />230 mg/L 100 0.54 MCAWW 200.7 08/12-08/13/03 FVON2ICW <br />Dilution Factor: 1 <br />Andl yeie Time..: 13:04 <br />(Continued on next page) <br />34 <br />