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MATRIX SPIRE, SAMPLH DATA REPORT <br />General Chemistry <br />Client Lot #_._: D3H080197 Matrix______.__: WATER <br />Date Sampled__.: 08/13/03 14:55 Date Received._: 08/13/03 <br />SAMPLE SPIKE MEASRD ~ PERCNT PREPARATION- PREP <br />PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE BATCH d. <br />Ammonia as N WO#: FVWCDIAH-MS/FVWCDIAJ-MSD MS Lot-Sample #: D3 H070396- 005 <br />ND 4 .00 4.15 mg/L 103 MCAWW 350.1 08/15/03 3228206 <br />ND 4. 00 4.14 mg/L 103 0.26 MCAWW 350.1 08/15/03 322820E: <br /> Dilution Factor: 1 <br /> -- ~-~- Analysis Time..: 15:00 -' ~ - <br />Chloride WO#: FVW991D0-MS/F'VW991D1-MSD MS Lot-Sample #: D3 H080182- 001 <br />4.4 50.0 54.7 mg/L 101 MCAWW 325.2 08/18/03 3230240 <br />4.4 50.0 53.7 mg/L 99 1.8 MCAWW 325.2 08/18/03 323024p <br /> Dilution Factor: 1 <br />' Analysis Time..: 15:00 ' <br />Fluoride WO#: FVOPGICE-MS/FVOPGICF-MSD MS Lot-Sample #: D3H080357- 003 <br />0.89 5. 00 6.01 mg/L 102 SM 18 4500-F C 08/22/03 323448f~ <br />0.89 5. 00 5.87 mg/L 100 2.5 SM 18 4500-F C 08/22/03 323448f: <br /> Dilution Factor: 1 <br /> Analysis Time..: 16:00 ' <br />Fluoride WO#: FV3VOICP-MS/FV3VOICQ-MSD MS Lot-Sample #: D3H110207- 001 <br />0.90 5. 00 6.27 mg/L 107 SM18 4500-F C 08/22/03 3234487 <br />0.90 5. 00 6.27 mg/L - 107 0.0 SM18 4500-F C 08/22/03 323448"i <br /> Dilution Factor: 1 <br /> Analysis Time..: 16:00 <br />Fluoride WO#: FV8A31CN-MS/FVBA3ICP-MSD MS Lot-Sample #: D3H130327- 002 <br />0.99 5. 00 6.35 mg/L 107 SM18 4500-F C 08/22/03 3234485 <br />0.99 5. 00 6.29 mg/L 106 0.83 SM 18 4500-F C 08/22/03 323448°. <br /> Dilution Factor: 1 <br /> Analysis Time.-: 16:00 <br />Nitrate-Nitrite WO#: FVT371CM-MS/FVT371CN-MSD MS Lot-Sample #: D3H070280- 001 <br />0.023 4. 00 3.70 mg/L 92 MCAWW 353.2 08/15/03 3228216 <br />0.023 4. 00 3.81 mg/L 95' 2.8 MCAWW 353.2 08/15/03 3228216 <br /> Dilution Factor: 1 <br /> Anal ysie Time..: 15:00 <br />Nitrate-Nitrite WO#: FWAXIIAJ-MS/FWAXIIAK-MSD MS Lot-Sample #: D3 H140348- 012 <br />ND 4. 00 3.38 mg/L 85 MCAWW 353.2 08/18/03 3231439 <br />ND 4. 00 3.35 mg/L 84 0.89 MCAWW 353.2 08/18/03 323143° <br /> Dilution Factor: 1 <br /> Analysis Time..: 18:00 <br />(Continued on next page) <br />56 <br />