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MATRIR SPIKB SAMPLH SVALDATION REPORT <br />TOTAL Metals <br />Client Lot # ...: D4G090452 Matrix.........: WATER <br />Date Sampled ...: 07/09/04 13:25 Date Received. .: 07/09/04 <br /> PERCENT RECOVERY RPD PREPARATZON- WORK <br />PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE ORDER # <br />Nickel 99 (90 - 110) MCAWW 200.7 07/14-07/15/04 GKTMOIC2 <br /> 102 (90 - 110) 3.3 (0-20) MCAWW 200.7 07/14-07/15/04 GKTMOIC3 <br /> Dilution Factor: 1 <br /> Analysis Time..: 13:17 <br />Potassium 109 (86 - 111) MCAWW 200.7 <br />114 N (86 - 111) 3.4 (0-20) MCAWW 200.7 <br />Dilution Factoz: 1 <br />Analysis Time..: 17:33 <br />Sodium NC,MSB (91 - 112) MCAWW 200.7 <br />NC,MSH (91 - 112) (0-20) MCAWW 200.7 <br />Dilution Factor: 1 <br />Analysis Time..: 17:33 <br />Calculations are Performed before rounding [o avoid rowM-off errors in calculated results. <br />N Spiked analyte recovery is outside stated control limits. <br />NC 'the recovery aM/or RPD were nol calculated. <br />MSB'Ii~e recovery and RPD were not calculatM because fie sample amount was greatu Nan four rimes the spike amount. <br />07/14-07/19/04 GKTMOICR <br />07/14-07/19/04 GKTMOICT <br />07/14-07/19/04 GKTMOICO <br />07/14-07/19/04 GKTMOICI <br />24 <br />