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LABORATORY CONTROL SAMPLE DATA RRPORT TOTAL Metals Client Lot #._.: D4G090452 Matrix.........: WATER SPIKE MEASURED PERCNT PREPARATION- WORK PARAMETER AMOUNT AMOUNT UNITS RECVRY METHOD ANALXSIS DATE ORDER # LCS Lot-Sample#: D4G 130000-374 Prep Hatch #... : 4195374 Aluminum 2.00 2.12 mg/L 106 MCAWW 200.7 07/14-07/19/04 GK0611AN Dilution Factor : 1 Analysis Time.. : 17:19 Calcium 50.0 51.3 mg/L 103 MCAWW 200.7 07/14-07/19/04 GK0611AP Dilution Pactor : 1 Analysis Time.. : 17:19 Cadmium 0.0500 0.0500 mg/L 100 MCAWW 200.7 07/14-07/15/04 GK0611AQ Dilution Factor: 1 Analysis Time.. : 11:14 Chromium 0.200 0.204 mg/L 102 Dilution Factor: 1 MCAWW 200.7 07/14-07/15/04 GK0611AR Analysis Time..: 11:14 Iron 1.00 0.998 mg/L 100 Dilution Factor: 1 Potassium 50.0 50.1 mg/L 100 Dilution Factor: 1 Magnesium 50.0 51.5 mg/L 103 Dilution Factoz: 1 Manganese 0.500 0.509 mg/L 102 Dilution Factor: 1 Sodium 50.0 52.8 mg/L 106 Dilution Factor: 1 Nickel 0.500 0.504 mg/L 101 Dilution Factor: 1 Beryllium 0-0500 0.0513 mgjL 103 Dilution Factor: 1 MCAWW 200.7 07/14-07/16/04 GK0611AT Analysis Time..: 14:91 MCAWW 200.7 07/14-07/19/04 GK0611AU Analysis Time..: 17:19 MCAWW 200.7 07/14-07/19/04 GK0611AV Analysis Time..: 17:19 MCAWW 200.7 07/14-07/15/04 GK0611AW Analysis Time..: 11:14 MCAWW 200.7 07/14-07/19/04 GK0611AX Analysis Time..: 17:19 MCAWW 200.7 07/14-07/15/04 GK0611A0 Analysis Time..: 11:14 MCAWW 200.7 07/14-07/19/04 GK0611A1 Analysis Time..: 17:19 LCS Lot-Sample#: D4G150000-233 Prep Batch #...: 4197233 Zinc 0.0400 0.0426 mg/L. 106 MCAWW 200.8 07/20-07/21/04 GK5DPIAJ Dilution Factor: 1 Analysis Time..: 20:26 Silver 0.0400 0.0406 mg/L 101 MCAWW 200.8 07/20-07/21/04 GKSDPIAK Dilution Factor: 1 Analysis Time..: 20:26 (Continued on next page) 19