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~C09E~I CORE LABORATORIES D U A L I T Y C O N T R O L R E S U L T S Job Number.: 983261 Repor[ Date.: 12/29/98 CUSTOMER: Greystone PROJECT: OTRY 484-03 Castillo Cnty ATTN: Nick Ma [his Test Method........: EPA 150.1 Batch ........ .....: 42046 Analyst...: mjf Method Description.: pN Units ........ .....: pN Units Test Code.: PH Parameter..........: pH OL Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result • Limits Dale Time MD 983248-1 7.85 7.84 0.1 R 20 12/10/1998 1435 CCV 980265 7.01 7.00 100.1 X 90-110 12/10/1998 1435 ICV G980923Z 4.04 4.00 101.0 X 90-110 12/10/1998 1435 Test Method........: EPA 204.2 Batch .............: 42191 Analyst...: lmt Method Description.: Antimony (GFAA) Units .............: mg/L Test Lode.: SB Parameter..........: Antimony (Sb) OL Lab ID Reagent DC Result 0C Result True Value Orig. Value Lalc. Result ' Limits Date Time ICV 981214V 0.04301 0.0400 107.5 % 90-110 12/14/1998 1438 ILB 12148 0.00006 0.002 12/14/1998 1441 MB 1207 0.00011 0.002 12/14/1998 1444 EB 1202 0.00194 0.002 12/14/1998 1448 SB 980826) 0.02130 0.020000 106.5 % 80-120 12/14/1998 1451 MS 983093-1 980826) 0.02110 0.020000 0.00218 94.6 X 75-125 12/14/1998 1457 MSD 983093-1 980826) 0.02187 0.02110 0.020000 0.00218 98.5 % 75-125 12/14/1998 1501 3.6 R 20 ED 983093-1 0.00301 0.00218 0.00083 A 0.00200 12/14/1998 1504 SD 983093-1 0.00082 0.00218 12/14/1998 1507 MB 1211 -0.00012 0.002 12/14/1998 1510 CCV 981214C 0.04768 0.050000 95.4 % 90-110 12/14/1998 1513 LLB 12148 -0.00069 0.002 12/14/1998 1517 SB 980826) 0-02160 0.020000 108.0 % 80-120 12/14/1998 1520 MS 983271-1 980826) 0.01694 0.020000 -0.00037 86.5 % 75-125 12/14/1998 1526 MSD 983271-1 980826) 0.01714 0.01694 0.020000 -0.00037 87.5 % 75-125 12/14/1998 1529 1.2 R 20 SD 983236-3 -0.00001 0.00008 12/14/1998 1536 MB 1209 -0.00028 0.002 12/14/1998 1539 SB 980826) 0.01851 0.020000 92.5 % 80-120 12/14/1998 1542 CCV 981214C 0.04973 0.050000 99.5 % 90-110 12/14/1998 1549 CCB 12148 0.00133 0.002 12/14/1998 1552 MS 983186-1 980826) 0.01912 0.020000 0.00099 90.7 Y. 78-125 12/14/1998 1555 MSD 983186-1 980826) 0.01890 0.01912 0.020000 0.00099 89.5 % 75-125 12/14/1998 1558 1.2 R 20 PDS 983261-1 981214G 0.02051 0.020000 -0.00008 103.0 X 75-125 12/14/1998 1608 PSD 983261-1 981214G 0.02090 0.02051 0.020000 -0.00008 104.9 % 75-125 12/14/1998 1611 1.9 R 20 SD 983261-1 -0.00066 -0.00008 12/14/1998 1615 LLV 981214C 0.05034 0.050000 100.7 % 90-110 12/14/1998 1618 CCB 12148 0.00074 0.002 12/14/1998 1621 Test Method........: EPA 200.7 Batch .............: 42373 Analyst...: lmt Method Description.: Metals Anal ysi s(ICAP ), Trace Units .............: mg/L Test Code.: AS Parameter..........: Arsenic (AS) OL Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result • Limits Date Time LRA 9812080 -0.00174 12/16/1998 1126 LRA 981008M -0.00080 12/16/1998 1129 LRA 981203M -0.00194 12/16/1998 1134 Page 6 ' %_% REC, R=RPD, A=ABS Diff., D=% Diff. i ~mo ~...a.~o.,~ti-,_..~o.a~.~.~.~~,.~a,~o~.,,~ro...~-.~m~..,,.,.~,,.,.o.,.~-~~N.o.~~...~.~.~..,~~w.~.~,,.M~.~,~~o~a~.o.~,..,...~.a,..,..,.~,,,~. ~~,,,~,~,.~~~~~~, ~.,.. o,~„