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I~MG~Bj <br />CORE LABORATORIES <br />Q U A L I T Y C O N T R O L R E S U L T S <br />Job Number.: 983261 Report Date.: 12/29/98 <br />CUSTOMER: Greys tone PROJECT: OiRY 484-03 Castillo Lnty ATTN: Nick Mathis <br />Test Method........: EPA 270.2 Batch .............: 42188 Analyst...: lmt <br />Method Description.: Selenium (GFAA) Units .............: mg/L Test Lode.: SE <br />Parameter..........: Selenium (Se) <br />OC Lab ID Reagent DL Result DC Result True Value Orig. Value Calc. Result * Limits Date Time <br />CCV 981214A 0.04760 0.050000 95.2 % 90-110 12/14/1998 1300 <br />LCB 12148 -0.00063 0. 005 12/14/1998 1303 <br />CCV 981214A 0.04871 0.050000 97.4 % 90-110 1Z/14/1998 1307 <br />CCB 12148 -0.00147 0. 005 12/14/1998 1310 <br />LCV 981214A 0.04820 0.050000 96.4 Y. 90-110 12/14/1998 1317 <br />CCB 12148 -0.00117 0. 005 12/14/1998 1320 <br />Test Method........: EPA 200.7 Batch ........ .....: 42373 Analyst...: lmt <br />Method Description.: Metals Analysis([CAP ), Trace Units ........ .....: mg/L Test Lode.: AG <br />Parameter..........: Silver (Ag) <br />OL Lab ID Reagent QC Result OC Result True Value Orig. Value Calc. Result * Limits Date Time <br />LRA 9812080 0.99751 10.00 12/16/1998 1126 <br />LRA 981008M 0.00079 12/16/1998 1129 <br />LRA 981203M 0.00096 12/16/1998 1134 <br />LRA 981008E 0.00098 12/16/1998 1138 <br />LRA 981008K -0.00091 12/16/1998 1142 <br />LRA 981008K -0.00033 12/16/1998 1149 <br />ILV 9812161 0.50078 0.5 100.2 % 90-110 12/16/1998 1153 <br />ILV 9812161 0.50067 0.5 100.1 X 90-110 12/16/1998 1156 <br />[CB 9812168 0.00019 0.005 12/16/1998 1202 <br />ISB 981120M 1.01457 1.0002 101.4 % 80-120 12/16/1998 1210 <br />LCS 980865 0.34905 0.341000 102.4 Y, 74.5-125.8 12/16/1998 1224 <br />SB 9809295 0.04975 0.05 99.5 Y. 80-120 12/16/1998 1228 <br />CCV 981216[ 0.50543 0.5 101.1 X 90-110 12/16/1998 1256 <br />CCB 9812168 0.00023 0.005 12/16/1998 1300 <br />PDS 983261-1 9809295 0.04240 0.05 0.00025 84.3 % 75-125 12/16/1998 1332 <br />PSD 983261-1 9809295 0.04267 0.04240 0.05 0.00025 84.8 % 75-125 12/16/1998 1335 <br /> D.b R 20 <br />CCV 9812161 0.50077 0.5 100.2 % 90-110 12/16/1998 1340 <br />CCB 9812168 0.00034 0.005 12/16/1998 1348 <br />SD 983261-1 0.00074 0.00025 12/16/1998 1357 <br />MB 1216 0.00039 0.005 12/16/1998 1415 <br />56 9809295 0.05217 0.05 104.3 Y. 80-120 12/16/1998 1419 <br />LCS 980865 0.39666 0.341000 116.3 X 74.5-125.8 12/16/1998 1423 <br />CCV 9812161 0.45506 0.5 91.0 % 90-110 12/16/1998 1540 <br />CCB 9812168 0.00042 0.005 12/16/1998 1545 <br />CCB 9812168 0.00088 0.005 12/16/1998 1552 <br />ISB 981120M 0.91386 1.0002 91.4 % 80-120 12/16/1998 1632 <br />CCV 9812161 0.44988 0.5 90.0 % 90-110 12/16/1998 1636 <br />CCB 9812168 0.00018 0.005 12/16/1998 1640 <br />Page 14 <br />* %_% REC, R=RPD, A=ABS Diff., D=Y. Diff. <br />..~ ~...'.auo..,,~,,., a , . a~ . V„ m.. uvo„~o.,, a.,ro a.,,~.. ~,,.~,.. ~......o -.... , ~ „~..~~„e. ~~ ..,. m~ ~.~ ~~,m ~.« ,~~,...~.v, a. ~„m, gym.., , ,~~ o~mk,. ~, o o~. ao„„~ ~ ~.~.~.,o~~., , ~, <br />