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n u CORE LABORATORIES O U A L 1 T Y C O N T R O L R E S U L T S Job Number: 961500 Date: 06/25/96 LUSid1ER: Greysione ~. ~ ~ ~ ~ PROJECT: 464-03' ATTN: Ray Fac iski Test Method........:~EPA 270.2 ::. ~ ..~~.~ ~~~Batch........:.~:..:.:~9890 ..: :~. ~. ~ Analyst...: lmt Method~.Descri ption;: ~Sel enium (GFMT~ - .~ ~ Detection Liniif...: 0.005 ~~ Parameter..:..:.~::.:~:Sel;nium (Se)~..~~:~ :~::~~ ~ ~ ~ ~~ ~ ~UriF ts..~.:....::~.::: .>re/L. ~. OC Lab ID Reagent OC Result OC Result True Yalue Orig. Value Calc. ResulT Units F Date/Tine ICV 9604198 0.04121 0.0400 103.0 X REC 06/09/96 0900 - ICB 06106 0.00094 06/09/96 0906 CCV 9604260 0.04819 0.050 96.4 X REC 06/09/96 1004 CCB 06106 0.00026 06/09/96 1007 CCY 9604260 0.05123 0.050 102.5 X REC 06/09/96 1039 CCB 06106 0.00021 06/09/96 1042 MB 0607 0.00006 06/09/96 1059 LCS 96080bH 0.04252 0.040000 106.3 X REC 06/04/96 1102 MD 961492-1 0.00412 0.00630 0.00218 ABS Diff. 06/09/96 1109 MS 961490-2 960329G 0.01762 0.020000 0.00347 70.8 X REC 06/09/96 1118 MB 0605 -0.00109 06/09/96 1121 LCS 960424H 0.03934 0.040000 98.3 X REC 06/09/96 1124 CCV 9604260 0.05115 0.050 102.3 X 0.EC 06!09!% 1128 CCB 06106 0.00002 06/09/96 1131 MS 961477-1 960329G 0.02103 0.020000 0.00074 101.2 X REC 06/09/96 1137 MD 461477-1 -0.00010 0,00079 0.00089 ABS Diff. 06/09/96 1141 SD 961481-3 0.00044 0.00534 X Diff. 06/09/96 1147 [CV 9604260 0.04998 0.050 100.0 X REC 06/09/96 1150 CCB 06106 -0.00004 06/09/96 1153 CCV 9604260 0.05142 0.050 102.8 X REC 06/09/96 1255 CCB 06106 -0.00055 06/04196 1258 PDS 961490-2 9604010 0.02162 0.020000 0.00347 90.8 X REC 06/09/96 1302 CCV 9604260 0.05116 0.050 102.3 X REC 06/09/96 1305 CCB 06106 0.00010 06/09/96 1308 MD 961500-1 -0.00035 -0,00043 0.00008 ABS Diff. 06/09/96 1357 PDS 961500-2 9604010 0.01937 0.020000 -0.00024 98.0 X REC 06109!96 1404 SD 961500-3 -0.00033 -0.00058 X Diff. 06/09/96 1410 CCV 9604260 0.05252 0.050 105.0 X REC 06/09/96 1417 CCB 06106 -0.00030 06/09/96 1420 MB 0610 -0.00052 06/09/96 1439 LCS 960097 0.07523 0.072300 104.1 X REC 06109/96 1442 MS 961480-1 460329G 0.03548 0.020000 0,01559 99.5 X REC 06/09/96 1448 MD 961480.1 0.01553 0.01559 0.00006 ABS Diff. 06/09/96 1452 5D 961480-1 0.00242 0.01559 X Diff. 06109/96 1455 CCV 9604260 0.05406 0.050 108.1 X REC 06/09/96 1457 CCB 06106 -0.00089 06/09/96 1500 Test .Method..... ...: .EPA 335.2 Batch .............: 9902 ~ AnalYSt ...: kds Method Description .: Cyanide, Total (Tit., Spec.) Detection~ Limit...: 0.02 Parameter..........: Cyanide, Totat ~ Units .............: mg%l OC Lab ID Reagent OC ResulC OC Result True Value Orig. Value Calc. Result Units F Date/Time ICV G960209B 0.5475 0.500000 109.5 X REC 06/10/96 1800 ICB 0.0010 06/10/96 1800 DSC G960209C 0.2040 0.200000 102.0 X REC 06!10!46 1800 MB 0.0000 06/10/96 1800 MD 961438-1 0.0010 0.0005 0.0005 ABS Diff. 06/10/96 1800 MS 961438-1 G960209C 0.2334 0.250000 0.0005 93.2 X REC 06/10/96 1800 CCV G960209C 0.3019 0.300000 100.6 X REC 06/10/96 1800 CCB 0.0020 06110196 1800 Page 32 m..w,..~~.~.v.~.o.~.o.~i..a.~..e~..m~..am.m..e.~..~..m.ewa. n..~a.b..~a....a ,~~W W. ~... ~,ry. e..~m.d ~.~.M~,.~.,..m~,.o .~.a.~.~m. .o...e ,o.r, m. e~ ww~n m ce. ~e.~ w um.~. m..l. ~ m..,.,m a „~,..,.e,. w,., s,m.u m.., no..+e ..~.,., w..~. w... ~ ~. om....,.>oe. mr.~.... oo..o... n +m a. w. ca+> uir.... ww..r. w a wu ~~ «+w..m.~ w,.w... ~,.~+o.wi way ra.,h ~..u=... ^` ~"o+•^.• ^^~ n ~voa<c....v.> na....~ c..rnn uvaw m w...oom,~w