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C~E~ CORE LABORATORIES D U A L I T Y C O N T R O L R E S U L T S Job Number: 961500 Date: 0625!96 CUSTOMER: Greystone ~ ~ PROJECT: 484-03 ~ATTN: Ray Faciski Test Method....,..,: EPp 325.2 ~ Batch ....... .:....: 10152 ,. Mal ys t...: dte Method Description.:~ Chloride (COlori metric, M II) Detection Limi i~, ..: 0.5 Parameter-.........: Chloride .. Units ....:........: ~/! O[ Lab ID Reagent OC Result aC Result True Value Orig. Value Calc, Result Units F Date/Time CCV G960506E 83.31158 80.0 104.1 X REC 06/18/96 1500 - CCB 0.33187 06!18196 1501 LCS G960116A 52.28201 50,0 104.6 X REC 06/18/96 1504 CCV G960506E 81,85592 80.0 102.3 X REC 06/18/96 1517 CCB 0.33187 06!18196 1518 MD 961514-26 7.67890 7.55738 1.6 RPD 06/18/96 1530 MS 961514-26 G960506A 59.13941 50,000000 7.55738 103.2 X REC 06/18/96 1531 CCV G960506E 83.96894 80.0 105.0 X REC 06!18196 1534 CCB 0.33187 06/18/96 1535 LCS G960116A 53.40597 50.0 106.8 X REC 06/18/96 1537 CCV G960506E 81.25777 80.0 101.6 X REC 06/18196 1550 CCB 0,33187 06/18/96 1552 MD 961471-2 9.25806 9,05565 2.2 RPD 06/18/96 1558 MS 461471-2 G960506A 64.64594 50.000000 9.05565 111,2 X REC 06!18!46 1600 CCV G960506E 82.85826 80.0 103.6 X REC 06/18/96 1606 CCB 0.33187 06/18/96 1607 7 est~Method........: EPA 239.2 Batch .............: 10157 Analyst..,: lmt Method Description.: Lead (GFM) Detection Limit...: 0.002 Parameter..........: Lead (Pb) Units .............: mglL DC Lab ID Reagent OC Result oC Result True Value Orig. Value Calc. Result Units F Date/Time ICV 9604198 0.02015 0.020000 100.8 % REC 06!18!96 1141 ICB 06186 -0.000301 06/18/96 1153 CCV 9604260 0.02596 0.025000 103.8 Y. REC 06/18/96 1205 CC8 Ob186 0-001549 06/18196 1217 MD 961500-1 -0.000359 0.000071 0,00043 ABS Diff. 06/18/96 1241 POS 961500-2 9604010 0.01721 0.020000 -0,000645 89.3 % REC 06/18/96 1305 SD 961500-3 -0.000337 -0.000226 X Diff. 06!18/96 1329 MB 0605 -0,000304 06/18/96 1353 CCV 9604260 0.02356 0.025000 94,2 X REC Ob/18/96 1429 CCB 06186 -0.000127 06/18!96 1441 SD 961481.3 -0.000321 0.000024 X Diff. 06/18/96 1453 MD 961477-1 0.000126 -0.000357 0.00048 p85 Diff. 06/18/96 1518 MB 0607 0.000150 06/18/96 1542 MD 961492-1 0,000217 0.000283 0.00006 ABS Oiff. 06/18/96 1618 MS 961490-2 960329G 0.009988 0.020000 0.003541 32.2 X REC 06718!96 1642 CCV 9604260 0.02682 0.025000 107,3 X REC 06/18/96 1654 CCB 06186 -0.000119 06/18/96 1706 MS 961477-1 96D329G 0.02360 0.020000 -0.000357 119,8 X REC 06!18/96 1718 LCS 960606N 0.02395 0.020000 119.8 X REC 06/18/96 1730 LCS 960424N 0.02000 0.020000 100.0 % REC 06/18/96 1742 PDS 961490-2 9604010 0.01878 0.020000 0.003541 76.2 X REC 06/18!96 1754 CCV 9604260 0.02537 0.025000 101.5 X REC 06/18/96 1806 CCB 06186 -0.000867 06/18/96 1818 Page 24 m..w.~+...amw.w~r.rw.a. wrr...e. e. sm.. e.e wP.'m•nor.e~..rw.mna~n.u.nww...w,..~v mr~,r ww.roa wa..r w.o. mw.v. w..u. m..w+w r,.«wre.. .O~W'4 YI~.M 0~1 NN+ni olCV. lrvtlw~ (o.lAnww,.'aw. M~ N ~wv~M1 v ~p~wr.vn. W.u v nc.~ e1 VM1 r1w vc ,rmW rurY*. ,.n. ~ m W M1v.c+nY ww v~nev v wa nuW~~el ,ry p. y,. [al w oiMr rm~y. 4'cAn. A w vn N mrwclp• ~w MeA nO~ rvYr nrY]u M.C m.b Yry rWJn.ayrl~rl M rpYl ry bl Y rvNicE. n nyl v n pvl. MaI rn ~w mart d fo.IM.rw!