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<br />CORE LABORATORIES
<br />D U A L I T Y C O N T R O L R E S U L T S
<br />Job Number: 961500 Dete: 06/25/96
<br />CUSTOMER: GreYstone .. PROJECT: 484-03 ATiN: Ray Faciski
<br />Test. Method..,:..,,: EPA 420.1 ~ ~ ~~~ ~ .~~.~ ~~~~' `.. Bstch~.:..:-,. ,~.::..: 70028 ~. ~~~ Analyst.--: kds
<br />Method. Description,:Phenols, Totel. Recdverahle ~~ ~ Detection'L imit.~..: 0.05 .
<br />Parameter......:...: Pherm l,~Total Retovei•eble ~~:.~ ~.~ Un its.-..~, :.. .. ,..::.~mglL~~ ~~~~
<br />OC Lab ID Reagent 9C Result OC Result True Yalue Orig. Value Calc. Result Units F Dale/Time
<br />ICL 960067 0.0489 0.05 97.8 X REL 06/77/96 1900 _
<br />ICB -0.0018 O6{17/96 1900
<br />MB 0.0055 06(77/96 1400
<br />MD 961447-2 0.5979 0.5847 1.2 RPD 06/11/96 1900
<br />MS 961441-2 G951005A 0.7802 0.250000 0.5847 78.2 X REC 06/11/96 7900
<br />CCV G951005A 0.4905 0.500000 98.1 X REC 06!11/96 1900
<br />CCB -0,0076 06(11(96 1900
<br />Test Method........: EPA 375.2 Beteh .............: 10044 Analyst...: dire
<br />Method Description.: Sulfate (Automated XTB, AAii) Detection Limit...: 10.
<br />Parameter,,........: Sulfate (504) Units .............: mg/L
<br />DC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units F Date/Time
<br />ICL G951103A 49.13860 50.0 98.3 X REC 06/13/96 7545
<br />ICa -1.85535 06/13/96 7547
<br />ND 967467-1 10.71785 70.54440 0.17345 ABS Dift, 06113!96 1552
<br />NS 961467-7 G960670A 60,62757 50.000000 10.54440 100.2 X REC 06/13/96 7554
<br />ND 961494-7 -0.36932 7.28593 1.65525 ABS Diff. 06/73/96 1601
<br />CCV 4960415E 172.70492 120 93.9 X REC Ob/13)96 1608
<br />CCB -0.92493 06/13/96 1610
<br />LCS C951103A 48,69023 50.0 97.4 X REC 06/13/96 7627
<br />CCV 4960415E 111.30567 720 92.8 X REC 06/13/96 1631
<br />CCB -1,66882 06/13/96 1633
<br />ND 954817-249 1.83393 8.80105 6.96712 ABS Diff, 06(13!46 1638
<br />NS 954817-249 G960610A 59.02520 50.000000 8,80105 100.4 X REC 06/13/96 1640
<br />CCV 4960415E 110.74614 120 92.3 X REC 06/73/96 1654
<br />CCB -7,66882 Ob/ti/9b 1656
<br />CCV 4960415E 111.72531 120 93.1 X REC 06/13(96 1717
<br />CCB -1,66882 06/13/96 1779
<br />ND 961375-16 194,33641 185.81377 4.5 RPD 06/13/96 1728
<br />CCV 4960475E 727,26666 120 701,1 % REC 06/13/96 1740
<br />CCB -0,18455 06/73/46 1742
<br />LCS G951703A 49.58644 50.0 99.2 X REL 06/73/96 7800
<br />CCV 4960415E 118.77274 120 98,5 X REC 06/13/96 1803
<br />CCB -1,66882 06/13/96 1805
<br />ND 961375-28 32,76531 31.18850 7.57681 ABS Diff. 06/13/96 1809
<br />NS 961375-28 C960670A 77.96436 50.000000 31.18850 93.6 X REC 06/13/96 7870
<br />CCV 4960415E 124,65782 120 103.9 X REC 06/73/96 7826
<br />CCB 4,36757 06!73196 1828
<br />Test Method.....,.,: EPA 204.2 Baich .............: 10077 Analyst,..: Imt .
<br />Method Description.: Antimony (GFAA) Oetec tion Limit...: 0.002 ,
<br />Parameter.........,: Antimony (Sb) Units .............: mg/L
<br />OC Lab ID Reagent OC ReSUIt OC Result True Value Orig, Value Calc. Result Units F Date/Time
<br />ICV 9606148 0.04399 0.0400 110.0 X REL 06/14/96 1006
<br />ICB 06146 -0,00092 06/14/96 1013
<br />CCV 960614[ 0,05043 0.0500 100.9 X REC 06/14/96 1043
<br />CCB 06146 -0,00203 06!14/46 1047
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