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Metals by 200.8 <br />Method EPA200.8 Revision 5.4 <br />Matrix Spike And Matrix Spike Duplicate <br />Lab Name: Paragon Analytics <br />Work Order Number: 0509140 <br />Client Name: CEMEX, Inc. <br />ClientProject ID: A+c Pits <br />I~Ij§y.~e a°nxae`am~em44nam°f SampleMatrix:WATER Prep Batch:IP050930-22 Sample Aliquot: 50g <br />e1d,ID•3~A-PIT Th 8 Se <br />i+y'L'i}Ig~ I % Moisture: N/A gCBatchID: IP050930.22-1 Final Volume: 50g <br />ablD~ 0509140-1M5 <br />.,a~a......__..._..._....®._,,. Date Collected: l6-Sep-05 Run lD:im050930-1 a2 Result Units: ug/I <br />Date Extracted: 30-Sep-OS Cleanup: NONE File Name: 30SEPOSA <br /> Date Analyzed:30-Sep-OS <br />Prep Method: EPA2002 Basis: As Received <br /> <br />CASNO TargetAnalyte Sample Samp <br />Result Qual MS MS Reporting <br />Result Qual Limk Spike MS% <br />Added Rec. Control <br />Limits <br />7762-49-2 SELENIUM 2 43.6 1 40 104 70-130% <br />7440-28-0 THALLIUM 0.2 1.02 0.2 1 102 70 - 130 <br /> <br />4^'WiR'!II' LNb3b <br />a`~° ~ ~ ~ Sample Matrix:WATER <br />Fie D A-PIT Th 8 Se <br />Moisture: N/A <br />LID• 0509140iMSD~~ <br />;mum-~ _ Date Collected: i6-Sep-OS <br />Date Extracted:30-Sep-O5 <br />Date Analyzed: 30-Sep-OS <br />Prep Method: EPA200.2 <br />Prep Batch: IP050930-22 <br /> <br />pCBatchlD: IP050930-22-1 <br /> <br />Run lD:im050930-1 a2 <br />Cleanup: NONE <br />Basis: As Received <br />Sample fdlquot: 50g <br /> <br />Final Volume: 50g <br /> <br />Result Units: ug/I <br />File Name: 30SEP05A <br /> <br />CASNO Target Analyte MSD MSD <br />Result Qual Spike MSD% Reporting <br />Added Rec. Limit RPD RPD <br />Limit <br />7762-49-2 SELENIUM 41.2 40 96 1 20 6 <br />7440-26-0 THALLIUM 127 1 127 0.2 20 21 <br /> <br />Data Package ID: im0509140-1 <br />Date Printed: Wednesday, October 12, 2005 Paragon Analytics Page 1 of i <br />LIMS V°rslon: 5.244A <br />17 <br />