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<br /> <br /> <br />CORE LABORATORIES <br />Q U A L I T Y C O N T R O L R E S U L T S <br />Job Number: 980539 Dale: 03/25/98 <br />CUSTOMER: Creystone PROJECT: COSTILLA CNTY 484-03 ATTN: Nick Ma[his <br />Test Method-.......: EPA 200.7 Batch ..... ........: 32566 Malyst...: lmt <br />Method Description.: Metals Anal ysis(ICAP), Trace Units .............: mg/L <br />Parameter..........: Barium (Ba) <br />OC Lab ID Reagen[ DC Result OC Result True Value Orig. Value Calc. Result ' Limits Date/Time <br />ICV 980312V 5.08009 5.0 101.6 X 90-110 03/24/98 1107 <br />[CB 9803168 0.00027 0.001 03/24/98 1117 <br />ISB 980311U 0.99985 1.000 100.0 X BO-120 03/24/98 1130 <br />SD 980723-1 0.01112 0.05316 -4.6 D -10.0-10.0 03/24/98 1151 <br />CCV 980312V 5.09399 5.0 101.9 X 90-110 03/24/98 1230 <br />CCB 9803168 0.00068 0.001 03/24/98 1233 <br />CCV 980312V 4.98772 ~ S.D 99.8 X 90-110 03/24/98 1308 <br />CCV 980312V 4.91456 5.0 98.3 X 90-110 03/24/98 1319 <br />CCB 9803168 0.00041 0.001 03/24/98 1325 <br />PDS 970111-59 9803195 1.00218 1.000 0.00695 99.5 X 75-125 03/24/98 1331 <br />PSD 970111-59 9803195 0.99912 1.00218 1.000 0.00695 99.2 X 75-125 03/24/98 1334 <br /> 0.3 R 20 <br />ISB 980311U 0.95469 1.000 95.5 X 80-120 03/24/98 1359 <br />CCV 980312V 4.85651 S.D 97.1 X 90-110 03/24/98 1405 <br />Test Method........: EPA 200.7 Batch .............: 32566 Malyst...: lmt <br />Method Description.: Metals Anal ysi s(ICAP), Trece Unite .............: mg/L <br />Parameter..........: Iron (Fe) <br />OC Lab ID Reagent DC Resul[ OC Result True Value Orig. Value Calc. Result ' Limits Dale/Time <br />ICV 980312V 10.39352 10.0 103.9 X 90-110 03/24/98 1107 <br />ICB 9803168 0.01307 0.03 03/24/98 1117 <br />ISA 9803115 96.74494 100.00 96.7 X 80-120 03/24/98 1126 <br />ISB 980311U 94.83914 100.00 94.8 X 80-120 03/24/98 1130 <br />SD 980723-1 0.03785 0.10129 D 03/24/98 1151 <br />CCV 980312V 10.58817 10.0 105.9 X 90-110 03/24/98 1230 <br />CCB 9803168 0.02383 0.03 03/24/98 1233 <br />CCV 980312V 10.70214 10.0 107.0 X 90-110 03/24/98 1308 <br />CCV 980312V 10.61081 10.0 106.1 X 90-110 03/24/98 1319 <br />CCB 9803168 0.02392 0.03 03/24/98 1325 <br />PDS 970111-59 9803195 1.09273 1.0000 0.01673 107.6 X 75-125 03/24/98 1331 <br />PSD 970111-59 9803195 1.08631 1.09273 1.0000 0.01673 107.0 % 75-125 03/24/98 1334 <br /> 0.6 R 20 <br />ISA 9803115 99.58997 100.00 99.6 X 80-120 03/24/98 1356 <br />158 980311U 96.24201 100.00 96.2 X 80-120 03/24/98 1359 <br />CCV 980312V 10.54765 10.0 105.5 X 90-110 03/24/98 1405 <br />CCB 9803168 0.01289 0.03 03/24/98 1408 <br />Test Method........: EPA 200.7 Batch .............: 32566 Analyst...: lmt <br />Me[hod Descri p[ion.: Metals Malysis(ICAP), Trece Units .............: mg/L <br />Parameter..........: Lead (Pb) <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Lalc. Result ' Limits Dale/Time <br />ICV 980312V 2.51891 2.5 100.8 X 90-110 03/24/98 1107 <br />ICB 9803169 -0.00113 0.003 03/24/98 1117 <br />ISB 980311U 0.99232 1.000 99.2 X 80-120 03/24/98 1130 <br />SD 980723-1 -0.00001 0.00229 D 03/24/98 1151 <br />CCV 980312V 2.56722 2.5 102.7 X 90-110 03/24/98 1230 <br />CCB 9803168 0.00035 0.003 03/24/98 1233 <br /> Page 5 <br /> X-X REC R-RPD A-ABS Diff. D-X Diff. <br /> ....,~r..r....rr.~..o~.,,r.r,.a.r.rv,Tr,~.~,~~,.~r,w.~,.a~~r.re,m.b..,r•am.r...r~,o~.a mrr.d.•r rer_r~....~~....~a.~.r~..r..r ~.. r~, .o..~m~.~~..w~~. r.,~rr. o~..~. o <br />..o.wo ..r~•.., m.~r r•.wmtir or :.,...w..ro.,. ce.. uo>.r<.,.. •n...w ...e r„...•..r,n o r~rawr.re~ ..a,~. ar ma.e o~.r...o. w..o.... a«~.+.•. ~... ro ,,. oreo.~~«r. o w. orr.r.a.. o r..r..>.r,.~•, <br />o,oe,or.•....r <br /> c. or Yf .d ryrn mvc orcon, wrrv•n wmcm++rrn.rrn wm i.wnw•~n.ru mrrd yy rcon.rr.yc.rw ivrw~vy mrc.r.vm`~.,n«..yv~n vn «mm~rrr, w..nw..OVOw ar Cn ,uw'.rwu <br />