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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />.- .. <br /> <br />L43879-03 WG165836 Calcium, dissolved M200.71CP M3 The accuracy of the spike recovery value is reduced since <br /> the analyle concentration in the sample is disproportionate <br /> to spike level. The method control sample ewvery was <br /> • acceptable. <br /> Magnesium, tlissolved M200.71CP PMM One spike rewvery was outside of [he method limits; the <br /> duplicate spike and the method wntrol recoveries were <br /> within the method limits. <br /> Manganese, tlissolved M200.7 ICP kM One spike recovery was outside of the method limits; the <br /> duplicate spike antl the methotl control recoveres were <br /> within [he method limits. <br /> Zinc, dissolvetl M200.7 ICP kM One spike recovery was outside of the method limits; the <br /> duplicate spike and the method control recevedes were <br /> within the methotl limits. <br />WG165720 NitmteMitrhe as N, tlissolvetl M353.2 -AUtomatetl Cadmium F6 Sample was rer»ivetl antl analyzetl past holtling time. <br /> Reduction <br />WG165631 Nitrate as N, dissolved M353.2 -Automated Catlmium F6 Sample was receivetl antl analyzed past holtling time. <br /> Retluclion <br />L43679-06 WG165836 Calcium, dissolved M200.7 ICP M3 The accuracy of the spike recovery value is reduced since <br /> the analyte concentration in the sample is disproportionate <br /> to spike level. The method control sample recovery was <br /> acceptable. <br /> Magnesium, dissolved M200.71CP PAA One spike recovery was outsitle of [he methotl limits; the <br /> duplicate spike and the method control recoveries were <br /> within the method limits. <br /> Manganese, dissolved M200.7 ICP kM One spike recovery was outside of the method limits; the <br /> duplicate spike and [he method control rewvedes were <br /> within the methotl limits. <br />WG165962 Sodium, dissolved M200.7 ICP BC Target analyte detected in calihration hlank at or above <br /> method reporting limd. Concentretion found in the sample <br /> was 20 times above the concentration found in the <br /> calibration blank. <br />WG165838 Zinc, dissolvetl M200.71CP kM One spike recovery was outsitle of the method limits; iha <br /> duplicate spike and the method control recoveries were <br /> within the method limits. <br />WG166720 Nitrate/Nitrate as N, dissolved M353.2 -Automated Cadmium Fi3 Sample was received and analyzed past holding time. <br /> Reduction <br />WG165631 Nitrate as N, di55olvetl M353.2 -Automated Cadmium W Sample was raceivetl and analyzed past holding lime. <br /> Reduction <br />EXT~UAL.11.20.02.01 <br />LA3879: Page 22 of 32 <br />Brown and Caldwell ACZ Project ID: L43879 <br />