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AL+Z Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 3345493 <br />Batch A distinct set of samples analyzed at a specific time <br />Fouts Value of the DC Type of interest <br />Limit Upper limi for RPD, in %. <br />Lower Lower Recovery Limit, in % (except far LCSS, mglKg) <br />MDL Method Detection Limi. Seine as Minimum Reporting Limit. Albws for instrument and annual fluctuations. <br />PCAVSCN A number assigned to reagents/standards !o trace to the manufacturer's certificate of arta)ysis <br />POL - Practical Duantitation Limit, typically 5 times the MDL. <br />QC Tme Value of the Control Sample or the amount added to the Spike <br />ReC Amount of the true value or spike added recovered, in % (except for LCSS, rrg/l(g) <br />RPD Relative Percent Difference, calculation used for Duplicate OC Types <br />Upper - Upper Recovery Limit, in % (except for LCSS, mgMg) <br />Serrrp'e - Value of the Sample o(interest <br /> <br />~ ~ f iyE4"'. j,,M"~X ,.' S '1 ~';,'P "t -.'' aj."v'!K'f" 4 Y'~ "Y ~- { S 1$a.r '.{,`~"a.'r <br />KS "~"Q° <br />yr,, ~ <br />' `'s <br />[ i <br />4~° <br />~{' -' <br />~i <br />~~ <br />a a. - <br />~ <br />T <br />` <br />~,' <br />' <br />~ ~" <br />` <br />~ <br />~ <br />- . <br />.~ <br />n t <br />2 <br />y o+..~' <br />~ <br />..ea..n.2.u c'x,t .... ..~'Si-,:_:..-.Sue- <br />r.u R`~ <br />mow:, <br />..>~.~:t.. , x <br />i <br />- <br />h <br />s^ <br />' ~.Y~ <br />+t.. <br />s <br />..u <br />..~` x ...,..t,z3.'~,~'..:1^c~v'~` ~~a <br />AS Analytical Spike (Post Digestion) LFM Labomtory Fortified Matrix <br />ASD Malytical Spike (Post Digestion) Duplicate LFMD Laboratory Fortified Matdx Duplicate <br />DUP Sample Duplicate LRB Laboratory Reagent Blank <br />LCSS Laboratory Control Sample -Soil MS/MSD Matrix Spike/Matrix Spike Duplicate <br />LCSW Laboratory Control Sample -Water PBS ~ Prep Blank -Soil <br />LFB Laboratory Fortified Blank P8W Prep 81ank -Water <br />GTrrE4Ti7T.1r7Ys!"5I ~,r*^r' .~^tw'X3S`~'i~ tTiw~4-s.~'ewS`~T `"..%~~Ls'~".x r^',;2?'<`Y t~~k~~f~~`"a+~...e'~.•...lF'~'i <br />Blanks Vedfies that there is no ar minimal contamunation in the prep method procedure. <br />Control Samples Verifies the accuracy of the method, induding the prep procedure. <br />Duplicates Verifies the Drecisbn of the instmment andlor rrethod. <br />SptkralFortified Matrix Determirres sample matrix interferences, i any. <br />B Analyte concentration detailed at a value between MDL and PDL. <br />H ~ Analysis exceeded method hold lima. pH is a field test with an immediate hold time. <br />R Poor spice recovery accepted because the other spike in the set fell within the given knits. <br />T High Relative Percent Difference (RPD) accepted because sample concentrations are less than 1(bc the MDL. <br />U Anayte was analyzed for but not detected at the indipled MDL <br />V High blank data accepted because sample concentration is 10 times higher than blank concentm6on <br />W Poor recovery (or Siver quaky control s accepted because Silver often precipitates with Chloride. <br />X Dualtry control sample is out of corrtrol. <br />Z Poor spike recovery is accepted because sample concentration s four times greater than spike ooncenlratan. <br />y.~> s-, - - .. .. ... <br />(1) EPA 600!4-83020. Methods for Chemical Analysis of Water and Wastes, March 1963, <br />(2) EPA 600/R-93100. Methods for the De[ertnination o(Inorganic Substances in Environmental Samples, August 7993. <br />(3) EPA 600IR-94-111. McMods for the Detertrina[ion of Metals in Environmental Samples - Supplerren[ I, May 1994. <br />(5) EPA SW-846. Test Methods for Evaluating Solid Waste, Thvd Ediion with Update III, Decertber 1996. <br />(6) Standard Methods for the Examination of Water and Wastewater, 19th edi'an, 7995. <br />• (1) DC results calwlated from raw data. Results may vary slightly if the rounded values are used in the calculations. <br />(2) Soil, Sludge, and Plant rretrices (or Inorganic analyses are reported on a dry weight basis. <br />(3) Animal matrices for Irorganic analyses are reported on an "as received" basis. <br />REPIN03.11.00.01 <br />L39081: Page 5 of I4 <br />