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ACiZ Laboratories, Inc. <br />2773 Doamhill Drive Steamboat Snrirms. CO 80487(800) 334-5495 <br />Wet Chemistry <br />- • . • • • • - ~ ivY:Ytii <br />akallrory as caco3 sMZ3zo6 - Titration <br />Bicarbonate ag sz6 mglL 2 20 03/13/07 0:00 caa <br />CaC03 <br />Carbonate as CaC03 71 mg0. 2 ZO 03/13/07 Ob0 eas <br />Hydroxide as CaC03 U mglL 2 20 03/13/07 0:00 cas <br />Trial Alkalirtily 587 mglL 2 20 03/13/07 Ob0 cas <br />Biochemical Oxygen M405.7 U • mglL 2 2 03/07/071221 Icp/ct <br />Demand (5 day) <br />CNoride M325.2 - Cdorimelric 7 ` mgll. 1 5 03/20/07 9:44 jag <br />Chranium, Hexavalent SM35000r-D 0.007 BH mglL 0.005 0.02 03/071071324 ct <br />Cyanide, total M335.4 - Colorimetrie w/ dactillatlon U mglL 0.005 0.03 03(19/07 13:56 nps <br />Cyanide, WAD SM4500-CN IL'olorimetric w/ U mglL 0.~5 0.03 03/16/07 10:54 1TF <br /> d~sblWfion <br />Fluoride SM4500F-C 12 mglL 0.1 0.5 03/1510713:11 cas <br />Hardness as CaC03 SM23406 - Calculatlon 15 mg/L 1 7 03/30/07 O:OD talc <br />Lab Filtration SM 3030 B 03!0710713:00 ct <br />tab FOtratlon 8 SM 3030 B ' 03/13/07 17:10 nYs <br />Acidiflra6ort <br />N'Nate as N, dissolved Calalalion: N03N02 minus N02 <br />0.30 <br />mglL <br />0.02 <br />0.1 <br />03!30/07 0:00 <br />talc <br />NltrateMitrite as N, M3532 -Automated Cadmium 0.36 H mglL 0.02 0.1 03/07/07 ?226 pjb <br />dissolved Reduction <br />Nitrite as N, dissolved M3532 - Autartiated Cadnrittm HU mglL 0.01 0.05 03107/072228 pjb <br /> Reduction <br />pH (lab) M150.7 - f-Jeetromefric <br />pH 6.9 H units 0.1 0.1 03/13(070:00 cas <br />pH measured at 21.0 C 0.1 0.1 03113!07 0'00 ras <br />Residue, Filterable M160.1 - Gtetdmetric 700 mg/L 10 ZO 03/08/07 15:43 Icp <br />(TDS) ~180C <br />Residue, NOn- M1602-Gravimetric 6 B ' mgfi_ 5 20 03109/0714:07 wpa <br />Fllterable (rSS) <br />~105C <br />SulfaGa SM4500 504-0 50 B • mg/1_ 10 50 03/09/07 11:39 wpa <br />Sulfide as S 3762 - Melttylene Blue U mg/L 0.02 0.7 03/07/07 15:19 cas <br />Note: Dissolved and total rtacoveraWe Copper values verified by re-analysis. <br />REPIN.02.06.05.01 'Please refer to Qualfier Reports Ior detail. <br />L61369: Page 5 of 21 <br />New Elk Mine ACZ Sample ID: 76138'9.01 <br />Project ID: pate Sampled: 03105107 15:00 <br />Sample ID: NEW-2 pate Received: 03/07/07 <br />Sample Matrix: Surface Water <br />