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1 <br />1 ~~I~ <br />CORE LABORATORIES <br />' 0 UAL I T Y C O N T R O L R E S U L T S <br />Job Nusber: 971377 Date: 06/30/97 <br />CUSTOMER: Greys[ane PROJECT: COST ILLA CO LANDFILL ATTN: Nick Mathis <br />Test Method........: EPA 335.2 Batch .............: 22293 Analysx...: lmj <br />I <br />Method Deseri pt ion.: Cyanide, Total (Tit., Spec.) Reporting Limit.. .: 0.02 <br />Parameter..........: Cyanide, Total Units ............ .: mq/t <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calt. Result Units Dete/Tine <br />' ICL G9611058 0.503 0.500000 100.6 X REC 06/04/97 1050 <br />ICB 0.000 06!04)97 1050 <br />DSC G961105A 0.206 0.200000 103.0 X REC 06/04/97 1050 <br />NB 0.000 06/04/97 1050 <br />' <br />MD 971377.1 0.000 0.000 0 ABS Diff. 06/04/97 1050 <br />MS 971378-3 G961105A 0.254 0.250000 0.000 101.6 X REC 06/04/97 1050 <br />CCV G961105A 0.292 0.300300 97.2 X REC 06/04/97 1050 <br />CC8 0.000 06/04/97 1050 <br />CCV G961105A 0.292 0.300300 97.2 X REC 06/04/97 1050 <br />CCB 0.000 06/04/97 1050 <br /> <br />Test Method........: EPA 279.2 Batch .............: 22311 Analyst...: lmt <br />Nethod Description.: Thallium (GFAA) Reporting Limit...: 0.005 <br />Perimeter..........: The Lliun (Tl) Units .............: mg/L <br /> <br />1 OC Leb ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Dete/Time <br /> ICV 970602B 0.04153 0.0400 103.8 X REC 06)04/47 1458 <br /> ICB 06047 -0.00049 06/04/97 1503 <br /> MD 971377-1 -0.00027 -0.00029 0.00002 ABS Diff. 06/04/97 1524 <br />' PDS 971377-2 970131H 0.02046 0.020000 -0.00036 104,1 X REC 06/04/97 1534 <br /> CCV 961202[ 0.05165 0.050 103.3 X REC 06/04/97 1545 <br /> CCB 06047 -0.00013 06/04/97 1550 <br />' CCV 461202[ 0.05255 0.050 105.1 X REC 06/04/97 1716 <br /> CCB 06047 -0.00049 06/04/97 1721 <br /> CCV 961202[ 0.05302 0.050 106.0 X REC 06/04/97 1748 <br /> CCB 06047 -0.00028 06/04/97 1753 <br /> <br />Test Method........: EPA 204.2 Batch .............: 22390 Analyst...: lmt <br />Method Description.: Antimony (GFAA) Reporting Limit...: 0.002 <br />Parameter..........: Antimony (Sb) Units .............: mg/L <br />OC Lab ID Reagent <br />~, ICV 9706028 <br />ICB 06057 <br />MD 971377-1 <br />PDS 971377-2 970514X <br />CCV 961202Y <br />CCB 06057 <br />OC Result OL Resuli True Value Orig. Value Calc. Result Units Date/Time <br />0.04345 0.0400 108.6 X REC 06/05/97 0924 <br />0.00020 06/05/97 0931 <br />-0.00025 0.00060 0.00085 ABS Diff. 06/05/97 0943 <br />0.02134 0.020000 -0.00086 111.0 X REC 06/05/97 0950 <br />0.05253 0.050000 105.1 X REC 06/05/97 0957 <br />0.00005 Ob/05/97 1001 <br /> Test Method........: EPA 245.1 Batch .............: 22448 Analyst...: veb <br /> Method Description.: Mercury (CVAA) Reporting Limit...: 0.0002 <br /> Parameter..........: Mercury (Hg) Units .............: nm/L <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time <br />ICV 961007G 0.004022 0.004000 100.6 X REC 06/06/97 1300 <br />ICB 06067 0.000002 06/06/97 1302 <br />MB 0605 -0.000010 06/06!97 1305 <br /> Page 26 <br /> <br />