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,1 <br />'~ LAB <br />CORE LABORATORIES <br />I 0 UAL I T Y C O N T R O L R E S U L T S <br />Job Number: 471377 Date: 06/30/97 <br />I CUSTOMER: Greys[one PROJECT: COSTILLA CO LANDFILL ATTN: Nick Mathis <br />1 <br />Test Method........: EPA 200.7 Batch .............: 22166 Mal yst...: smh <br />Method Description.: Metals Analysis(ICAP), Trace Reporting Limit...: 0.03 <br />Parameter..........: Iron (Fe) Units .............: mg/L <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Vel ue Calc. Result Units Date/Time <br />CCB 9702122 -0.01722 05/30!97 2359 <br />' Test Method........: EPA 200.7 Batch .............: 22766 Malyst...: smh <br />Method Description.: Metals Mal ysis(ICAP), Trace Reporting Limit...: 0.07 <br />Parameter..........: Manganese (NnI Units .............: mg/L <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time <br /> ICV 961106Y 2.08076 2.00 104.0 X REC 05/30/97 2016 <br /> ICB 9702122 0.00003 05/30/97 2059 <br /> ISB 970515% 0.43469 D.5000 86.9 % REC 05/30/97 2109 <br /> PDS 971377-1 970515U 0.98368 1.000 0.00044 98.3 X REC 05/30/97 2137 <br /> MD 971377-1 0.00036 0.00044 0.00008 ABS Di ff. 05/30/97 2145 <br /> CCV 970304Y 5.14240 5.0 102.8 X REC OS{30/97 2216 <br /> CCB 9702122 -0.00003 05/30/97 2227 <br /> CCV 970304Y 5.20650 5.0 104.1 X REC 05/30/97 2322 <br /> CCB 9702122 0.00003 05/30/97 2330 <br /> ISB 970515% 0.42400 0.5000 84.8 X REC 05/30/97 2343 <br /> CCV 970304Y 5.19509 5.0 103.9 X REC 05/30/97 2356 <br /> CCB 9702122 -0.00000 05/30/97 2359 <br />^ Test Nethad........: EPA 200.7 <br />I Method Descri ption.: Metals Analysis(ICAP), Trace <br /> <br />' Parameter.... <br />OC Lab ID ......: Nickel <br />Reagent (Ni) <br />OC Result OC Result <br /> ICV 961106Y 2.02954 <br /> <br />' ICB <br />ISB 9702122 <br />970515% 0.00019 <br />0.83983 <br /> PDS 971377-1 970515U 0.92549 <br /> MD 971377-1 -0.00003 <br /> CCV <br />CCB 970304Y <br />9702122 2.54458 <br />-0.00076 <br /> CCV 970304T 2.57255 <br /> CCB 9702122 -0.00002 <br /> ISB 970515% 0.83333 <br /> CCV 970304Y 2.56093 <br /> CCB 9702122 -0.00024 <br />1 <br />Batch .............: 22166 <br />Reporting limit...: 0.04 <br />Units .............: mg/L <br />True Value Orig. Value Calc. Result <br />2.00 101.5 <br />1.000 84.0 <br />1.000 -0.00043 42.6 <br />-0.00043 0.00040 <br />2.5 101.8 <br />2.5 102.9 <br />1.000 83.3 <br />2.5 102.4 <br />Malyst...: smh <br />Units De[e/Time <br />X REC 05/30/97 2076 <br />05/30/97 2059 <br />X REC 05/30/97 2109 <br />X REC 05/30/97 2137 <br />ABS Diff. 05/30/97 2145 <br />X REC 05/30/97 2216 <br />05/30/97 2227 <br />% REC 05/30/97 2322 <br />05/30/97 2330 <br />X REC 05/30/97 2343 <br />X REC 05/30/97 2356 <br />05/30/97 2359 <br />Test Method........: EPA 200.7 Batch .............: 22166 Analyst...: smh <br />Method Description.: Metals Analysi s(ICAP), Trace Reporting Limit...: 0.01 <br />Parameter..........: Silver (Ag) Units .............: mg/L <br />OC Lab ID Reagent OC Result OC Result True Yalue Orig. Value Calc. Result Units Date/Time <br />ICV 970325Y 2.09544 2.00 104.8 X REC 05/30/97 2031 <br />ICB 9702122 0.00409 05/30/47 2054 <br />ISB 970515% 0.88368 1.000 88.4 X REC 05/30/97 2109 <br />PDS 971377-1 970515U 0.91620 1.000 -0.00404 92.0 X REC 05/30/97 2137 <br /> Page 23 <br />1 <br />