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~p~L,~ CORE LABORATORIES ' 0 UAL I T Y C O N T R O L R E S U L T S Job Number: 971377 Dete: 06/30/97 I CUSTOMER: Greystone PROJECT: LOSTILLA CO LANDFILL ATTM: Nick Mathis t Test Method........: EPA 200.7 Batch .............: 22166 Malyst...: snh Me[hod Description.: Metals Analysis(iCAP ), Trace Reporting Limit...: 0.002 Parameter..........: Beryllium (Be) Units .............: mg/L OL Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time ' PDS 971377-1 970515U 1.03253 1.000 -0.00008 103.3 X REC 05/30797 2137 MD 971377-1 -0.00003 -0.00008 0.00005 ABS Diff. 05/30/97 2145 CLV 970304Y 2.52908 2.5 101.2 X REC 05/30/97 2216 CCB 9702122 -0.00008 05/30/97 2227 ' CCV 970304Y 2.55341 2.5 102.1 X REC 05/30/97 2322 CC8 9702122 0.00004 05/30/97 2330 ISB 970515X 0.47229 0.5000 94.5 X REC 05/30/97 2343 t CCV CCB 970304Y 9702122 2.57127 0.00004 2.5 102.9 X REC 05/30/97 05/30/97 2356 2359 Test Method........: EPA 200.7 Batch .............: 22166 Ana(yst...: snit Method Description.: Meals Analysi s(ICAP), Trace Reporting Limit...: 0.005 Parameter..........: Cadmi un (Cd) Units .............: mg/L OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time ICV 961106Y 2.02394 2.00 101.2 X REC 05/30/97 2016 ~ ICB 9702122 -0.00019 05/30/47 2059 ISB 970515% 0.85404 1.000 85.4 X REC 05/30/97 2109 PDS 971377-1 970515U 0.97269 1.000 -0.00004 97.3 X REC 05/30/97 2137 MD 971377-1 0.00024 •0.00004 0.00028 ABS Diff. 05/30/97 2145 ' CCV 970304Y 1.01605 1.0 101.6 X REC 05/30/97 2216 CCB 9702122 -0.00012 05/30/97 2227 CCV 970304Y 1.02496 1.0 102.5 X REC 05/30/97 2322 CCB 9702122 0.00014 05/30/97 2330 ' ISB 970515% 0.85371 1.000 85.4 X REC 05/30/97 2343 CCV 970304Y 1.01533 1.0 101.5 X REC 05/30/97 2356 CCB 9702122 0.00005 05/30/97 2359 ' OC Lab ID 1CY ICB ISA ' ISB PDS 971377-1 MD 971377-1 CCV CCB CCV CCB ISA ISB ' CCV CCB Test Method........: EPA 200.7 Batch .............: 22166 Analyst...: sah Method Oescri pt ion.: Metals Analysis(ICAP ), Trace Reporting Limit...: 5.0 Parameter..........: Calcium (Ca) Units .... .........: mg/L Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Dale/Time 9704102 103.08033 100.0 103.1 X REC 05/30/97 2049 9702122 -0.00969 05/30/97 2059 970418N 476.41238 500.0 95.3 X REC 05/30/97 2104 970515% 460.24572 500.0 92.0 X REC 05/30/97 2109 970515U 93.98377 50.000 46.26305 95.4 X REC 05/30/97 2137 45.99590 46.26305 0.6 RPD 05/30/97 2145 9704250 101.67358 100.00 101.7 X REC 05/30/97 2213 9702122 -0.00356 05/30/97 2227 9704250 101.21601 100.00 101.2 X REC 05/30/97 2316 9702122 0.03784 05/30/97 2330 970418W 483.48385 500.0 96.7 X REC 05/30/97 2340 970515X 454.46508 500.0 90.9 X REC 05/30/97 2343 9704250 95.69248 100.00 95.7 X REC 05/30/97 2351 9702122 0.04114 05130)97 2359 Page 21