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Metals by 200.8 <br />Method EPA200.8 Revision 5.4 <br />Matrix Spike And Matrix Spike Duplicate <br />Lab Name: Paragon Analytics <br />Work Order Number: 0512010 <br />Client Name: CEMEX, Inc. <br />ClientProject ID: <br />Field 1D: A-pit SE and Th Sample Matrix: WATER Prep Batch: IP051216-21 Sample Aliquot: 50 g <br />---^- • - ---- _ %Moisture:NIA pCBatchlD:fP051216-21-1 FinalVolume: 5Ug <br />LabID: 0512010-1MS Date Collectetl: 30-Nov-05 Run ID: IM0512161A3 Result Units: ug4 <br />Date Extracted: 16-Dec-05 Cleanup: NONE File Name: 16DE GOSA <br />Date Analyzed: 16-Dec-OS Basis: As Received - <br />Prep Method: EPA200.2 <br /> <br />CASNO TargetAnalyte Sample Samp MS MS Reporting Spike MS% Control <br />Result Qual Result Qual Limit Added Rec. Limits <br />77829-2 SELENIUM 3 39 1 40 90 70-130% <br />7440-2&0 THALLIUM 0.2 U ~ 1.24 0.2 1 124 70-130% <br /> <br />A pit SE and Th ~ - Sample Matrix: WATER <br />Field t0 <br />' Prep Batch: IP051216-21 Sample Aliquot: 50 g <br />, <br />------~-- - ----------- ~ - <br />: % Moisture: N/A QCBatchID:IP051216-21-1 Final Volume: 50g <br />-LabID :;0512010 1MSD Date Collected: 30-Now05 Run ID:IM051216-1A3 Result Units: ug/I <br />Date Extracted: 16-Dec-05 Cleanup: NONE File Name: 16DECOSA <br />Date Analyzed: 16-Dec-0S Basis: As Recaived <br />Prep Method: EPA200.2 <br /> <br />CASNO Target Analyte MSD MSD Spike MSD % Reporting RPD RPD <br />Result Qual Added Rec. Limit Limit <br />7762-09-2 SELENIUM 42.5 40 99 1 20 9 <br />7440-26-0 THALLIUM - }.26 1 126 0.2 20 2 <br /> <br />Data Package ID: 1M0512010-1 <br />Date Printed: Wednestlay, December 26, 2005 Paragon Analytics Page 1 of 1 <br />LIMS Version: 5.2B1A <br />11 <br />