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i ~ <br />C p~LAB CORE LABORATORIES <br />D U A L I T Y C O N T R O L R E S U L T S <br />Job Number: 973559 Date: 01/21/98 <br />CUSTOMER: Greystone PROJECT: COSTiLLA CO 484.05 ATTN: Nick Mathis <br />TesC Method........: EPA 239.2 Batch .............: 30246 Analyst...: lmt <br />Method Description.: Lead (GFAA) Units .............: mg/L <br />Parameter........--: Lead (Pb) <br />DC Lab !D Reagent OC Result OC Result True Value Orig. Value Calc. ResulT ' Limits Date/Time <br />PDS 973559-2 970811H 0.02475 0.020000 0.00229 112.3 X 75-125 01/15/98 0202 <br />PSD 973559-2 970811H 0.02395 0.02475 0.020000 0.00229 108.3 X 75-125 01/15/98 0209 <br /> 3.3 R 20 <br />CCV 971201C 0.05212 0.050 104.2 X 90-110 01/15/98 0240 <br />CCB 01148 0.00101 0.002 01f 15/98 0246 <br />Test Method........: EPA 340.2 Batch .............: 30257 Analyst...: Tlp <br />Method Description.: Fluoride (iSE) Unfits .............: mgfL <br />Parameter..........: Fluoride (F) <br />OC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. ResulC • Limi[s Date/Time <br />ICL G970506D 0.19 0.200000 95.0 X 90-110 01/15/98 0940 <br />ICB 0.00 0.1 01/15/98 0940 <br />LCS G970506D 1.85 2.000000 92.5 X 80-120 01/15/98 0940 <br />MD 973359-3 1.29 1.24 4.0 R 20 01/15/98 0940 <br />MS 973359-3 G980115B 2.22 1.000000 1.24 98.0 X 75-125 01/15/98 0940 <br />CCV G980115B 2.97 3.003003 98.9 X 90-710 01(15(98 0940 <br />CCB 0.00 0.1 01/15/98 0940 <br />Test Method........: EPA 200.7 Betch .............: 30331 Analyst...: gag <br />Method Description.: Metals Analysis(iCAP), Trace Unfits .............: mg/L <br />Parameter..........: Iron (Fe) <br />OC Lab ID Reagent OC Result DL Resu l[ True Value Orig. Value Calc. Result • Limi [s Date/Time <br />ICV 971219T 2.06526 2.00 103.3 X 90-110 01/18/98 1617 <br />ICB 9801078 -0.00479 0.03 01/18/98 1631 <br />ISA 971215W 98.13139 100 98.1 X 80-120 01/18/98 1639 <br />ISB 9712164 92.86259 100 92.9 X 80-120 01/18/98 1642 <br />ISB 971218W 1.87634 2.0000 93.8 X 80-120 01/18/98 1655 <br />PDS 980047-1 9711175 2.51289 2.0000 0.51484 99.9 X 75-125 01/18/98 1703 <br />PSD 980047-1 9711175 2.47524 2.51289 2.0000 0.51484 98.0 X 75-125 01/18/98 1705 <br /> 1.5 R 20 <br />CCV 971223V 5.19199 5.0 103.8 X 90-110 01/18/98 1721 <br />CCB 9801078 0.00716 0.03 01/18/98 1726 <br />SD 980047-2 0.01156 0.00526 D 01/18/98 1732 <br />CCV 971223V 5.04886 5.0 101.0 X 90-110 01/18/98 1806 <br />CCB 9801078 0.00655 O. D3 01/18/98 1813 <br />CCV 971223V 5.37268 5.0 107.5 X 90-110 01/18/98 1851 <br />CCB 9801078 0.00532 0.03 01/18/98 1905 <br />ISA 971215N 100.08354 100 100.1 X 80-120 01/18!98 1907 <br />ISB 971216N 95.26227 100 95.3 X 80-120 01/18/98 1910 <br />ISB 971218N 1.99675 2.0000 99.8 X 80-120 01/18/98 1919 <br />CCV 971223V 5.31505 5.0 106.3 X 90-110 01/18/98 1923 <br />CCB 9801078 0.00599 0.03 01/18!98 1934 <br />Page 7 <br />• X-X REC R-RPD A-ABS Diff. D-X Diff. <br />,na a~~T .a .nuu oo~nev ~r n v e e ~~cn .m an.e~ r..; iyn n e c..n gym.,, ~~v..f ~ a +. u[~c. ..r~~ s ~wm~.+ n.. i..v a.v ~~ ~i~a . • ~ n,., ..~..+~. ,~..w .rv.u ~', ~ ~~ -~p.~~.i ~..~ <br />e.Ora.w .eor~vn~ne u.r i.n~msm u!'na um.a i...~s. Ct.e ~co~. m....; rv~arv ..+n.:.....i....r. .. ~./.•eniai..~ e.[.~.. o. ^["+~ r..r ~~.. ~^a r.y..~..~.ii~~.., .. n..e .: iei in, mia... i~. n. ~. et~~ n... ~i~~i..., c..~~r..~i..~,. ~r <br />