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~~~~ CORE LABORATORIES Q U A L I T Y C O N T R O L R E S U L T S Job Number: 973559 Date: 01/21/98 CUSTOMER: Greystone PROJECT: COSTILLA CO 484.05 ATTN: Hick Mathis Tesx Method........: EPA 325.2 Batch .............: 3022D Analyst...: lmj Method Description.: Chloride (Colorimetric, AA 11) Units .............: mg/L Pa remeter..........: Chloride DC Lab ID Reagent OC Result OC Result True Value Orig. Value Cale. Result * Limits De[e/Time iCL G971209B 80.28391 80.0 100.4 X 90-110 01/14/98 1330 LCS G971209C 9.42098 10.0 94.2 X 80-120 01/74/98 1332 ICB 0.34753 0.5 01714!48 1333 MD 980076-1 24.16599 24.07332 0.4 R 20 01/14/98 1347 MS 980076-1 G970509A 74.88897 50.000000 24.07332 101.6 X 75-125 01114/98 1349 CCV G9710308 80.22516 80.0 100.3 X 90-110 01/14/98 1354 CCB 0.34753 0.5 01/14/98 1356 CCV G971030B 81.28517 80.0 101.6 X 90-110 01/14/98 1407 CCB 0.34753 0.5 01/14/98 1408 Test Method........: EPA 200.7 Batch .............: 30229 Analyst...: gag Nethod Description.: Metals Analysis(ICAP), Trace Units .............: mg/L Parameter..........: Barium (Ba) OC Lab ID Reagent OC Result OC Result true Value Orig. Value Cal c. Result • Limits Dale/Time ICV 971219V 2.04654 2.00 102.3 X 95-105 01/14/98 1709 ICB 9801078 -0.00011 0.001 01/14/48 1720 ISB 971216W 0.47892 0.5000 95.8 X BO-120 01/14/98 1738 ISB 971218H 1.00372 1.000 100.4 X 80-120 01114198 1748 CCV 971223V 5.04388 5.0 100.9 X 95-105 01/14/98 1853 CCB 9801078 0.00023 0.001 01/14/98 1901 CCV 971223V 5.07206 5.0 101.4 X 95-105 01/14/98 1959 CCB 9801078 -0.00014 0.001 01/14/98 2010 CCV 971223V 5.02980 5.0 100.6 X 95-105 01/14(98 210D CCB 9801078 -0.00017 0.001 01/14/98 2108 PDS 973559-2 9711175 1.01629 1.000 0.05905 95.7 X 75-125 01/14798 2315 PSD 973559-2 9711175 1.00814 1.01629 1.000 0.05905 94.9 X 75-125 01/14/98 2317 0.8 R 20 IS8 97121651 0.46033 0.5000 92.1 X 80-120 01/14/98 2322 IS8 971218N 0.97262 1.000 97.3 X 80-120 01/14/98 2328 CCV 971223V 4.94120 5.0 98.8 % 95-105 01/14/98 2336 CCB 9801078 -0.00017 0.001 01/14/98 2342 Test Method........: EPA 200.7 Batch .............: 30229 Analyst...: gag Method Description.: Metals Analysis(ICAP ), Trace Units .............: mg/L Pa remeter..........: Manganese (Mn) DL Lab ID Reagent OC Result OC Result True Value Orig. Value Lalc. Resin[ • Li mi [s Date/Time ILV 9712197 2.03081 2.00 101.5 X 95-105 01/14/98 1657 ICB 9801078 -0.00003 0-001 01/14/98 1720 I5B 971216(1 0.44395 0.5000 88.8 X 80-120 01/14/98 1738 ISA 971218% 45.61775 50.000 41.2 X BO-120 01114)98 1741 ISB 971218W 42.38136 51.000 83.1 X 80-120 01/14/98 1748 CCV 971223V 5.13684 5.0 102.7 X 95-105 01/14/98 1853 CCB 9801078 0.00029 0.001 01/14/98 1901 CCV 971223V 5.15707 5.0 103.1 X 95-105 01/14/98 1959 CLB 9801078 -0.00006 0.001 01/14/98 2010 CCV 971223V 5.10960 5.0 102.2 X 95-105 01/14/98 2100 CCB 9801078 -0.00013 0.001 01714798 2108 Page 5 ro ., ~, e.ov..n, .m...xnrrm re.ii ~ p ~nr rr Cri. un .~ror~.. Gr.e ~ni vn~r.e n~-..u. n..r • +.. a.. ~. ..o ~.~.~r.i~ . ..,... ` X-X REC R-RPD A-ABS Diff. D-X .. n~i n r.ii. ~. o. in..r ... ~ .~i n. ...~a.rn m o. r~.. r.n c~ w v.. n~x.u t.. Diff. r ao.~- ~~i