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WB8~1 CORE LABORATORIES DUAL I T Y C O N T R O L R E P O R T Job Number: 960720 Report Date: 04/02/96 CUSTOMER: Crays [one PROJECT: ATTN: Jeff Spi nzig Method......: EPA 270.2 Batch .............: 7464 Analyst,..: lmt Description.: Selenium (GFAA) Detection Limit...: 0.005 Parameter...: Selenium (Se) Unfits .............: mg/L OC La6 1D M Reagent OC Result True Value Orig. Value Alt. Value Calculation Result Analyzed ILV 9603018 0.04146 0.0400 X REC 103.7 03/27(96 1458 ICB 03276 0.00159 03/27/96 1504 MB 0325 0.00138 0387/96 1517 LCV 960301[ 0.04958 0.050 Y. REC 99.2 03/27/96 1621 CCB 03276 -0.00016 0387/96 1628 CCV 960301[ 0.05050 0.050 X REC 101.0 03/27/96 1726 CCB 03276 0.00021 03/27/96 1732 LCS 960214) 0.04504 0.040000 X REC 112.6 03/27/96 1739 MS 960701-1 T 4510160 -0.00034 0-002000 -0.00023 X REC -5.5 03/27/96 1757 MSD 960701-1 i 951016[ -0.00040 0.002000 -0.00023 -0.00034 % REC -8.5 0387746 1804 RPD -16.2 MD 960701-1 T 0.00002 -0.00023 ABS Difif. 0.00025 03/27/96 1810 POS 960701-1 7 9511190 0.01974 0.020000 -0.00023 Y, REC 99.8 03/27/96 1816 PSD 960701-1 7 9511190 0,01915 0.020000 -0.00023 0.01974 X REC 96.4 03727/96 1822 RPD 3.0 CCV 960301[ 0,05318 0.050 X REC 106.4 03/27/96 1829 CCB 03276 0,00012 03/27/96 1835 MD 960720-4 D 0,00002 0.00010 ABS Diff. 0.00008 03/27/96 1846 PDS 960740-1 D 9511190 0,04919 0.020000 0.03403 X REC 75.8 0387!96 1853 SD 960740-Z D 0.00721 0.03390 X Diff. 03/27/96 1859 CCV 960301[ 0.05179 0.050 X REC 103.6 03/27/96 1908 CCB 03276 0,00030 03/27/96 1914 CCV 460301[ 0,05314 0.050 X REC 106.3 03727/96 1959 CCB 03276 0.00019 03/27/96 2005 CCV 960301[ 0,05148 0.050 y. REC 103.0 03/27/96 2114 CCB 03276 -0.00058 03/27/96 2120 CCV 960301[ 0.04999 0.050 X REC 100.0 03/27/96 2229 CCB 03276 0.00012 0387!96 2236 MS 960749-1 5 951016[ 0.01663 0.020000 -0.00096 X REC 88.0 03/27/96 2332 MSD 960749-1 5 9510160 0,01595 0.020000 -0.00096 0.01683 X REC 84.5 03/27/96 2339 RPD 4.2 CCV 960301[ 0.04883 0.050 X REC 97.7 0387/96 2345 CCB 03276 -0.00009 03!27)96 2351 CCV 960301[ 0.04881 0.050 X REC 97.6 03/28/96 0010 CCB 03276 -0.00020 03/28/96 0016 Method.-....: EPA 340.2 Batch .............: 7493 Analyst...: o)ee Oescripti on.: Fluoride (ISE) Detection Limit...: 0.1 Parameter...: Fluoride (F) Unfits .............: mg/L OC Lab ID M Reagent DC Result Dil. Vat ue ICL G960216A 8.2 8.000000 LCS G960216A 0.2 0.200000 ICO 0.0 MS 960718-4 U G9602168 2.3 1.000000 MSD 960718-4 U G9602168 2.3 1.000000 CCV G960216B 5.1 5.000000 CCB 0.0 MD 960719-2 U 0.9 MD 960720-1 F 0.3 Orig. Value Aft. Value 1.2 1.2 2.3 0.9 D.3 Page 33 Calculation Resu li Analyzed X REC 102.5 03/27/96 1300 X 0.E[ 100.0 03/27/96 1308 03727196 1316 X REC 110.0 03/27!96 1357 X REC 110.0 03/27/96 1405 RPD 0.0 X REC 102.0 0387196 1445 0387796 1453 RPD 0.0 03/27/96 1517 ABS Diff. 0.0 03/27/96 1533 ~.,.,~......~, m.a. v ~~.o..m.~,..e-,m,.m,.. d,o ~,.~-.~a.4 ~.~..~ a ~.....,~ ~..b....a„..b ~,. W.,~,~, w ~ ~ ~...,..~.. ~..,... m..o.. s.,~.o...o. .,> y.. m, s ~..~.. ~,. .. s..e., m....m.,...,a ,a,,.w., ~>.~,m.. u....~..~ ,~. ,.om .~. p~ d b~ ~.~ o. o.,....~.....~,~~ m.. s ca. ~..~