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~C~E~'. CORE LABORATORIES Q U A L I T Y C O N T R O L R E P O R T Job Number: 960720 Report Date: 04/02/96 CUSTOMER: Greys tone PROJECT: ATTN: Jeff Spinxig .~ Method......: EPA 200.7 8axch .............: 7412 Anel yst...: gef~ Description.: Metals Analysis(IGP), Trace Detection Limit...: 0,01 Parameter...: Manganese (Mn) Units .............: mg1L OC Lab ID M Reagent OC Result True Value Orig. Value Aft. Value Calculation Resul[ Analyzed ICV 9603122 1.43090 2.00 X REC 96.5 03{26196 1856 ICB 9603057 -0.00018 03/26/96 1942 ISB 9602297 0,42834 0.5000 X REC 85.7 03!26196 2008 CCY 9602167 4.87395 5.0 X REC 97.5 03!26!96 2047 CCB 9603057 0,00037 03/26/96 2103 LCV 9602167 4,93083 5.0 X REC 98.6 03/26/96 2154 CCB 9603057 0,00009 03/26/96 2209 MD 960720-2 D 0.03808 0.03761 ABS Diff. 0.00047 03/26/96 2216 PDS 960720-2 D 960228% 0,91353 1.000 0.03761 X REC 87.6 03/26/96 2224 CCV 9602167 4.92449 5.0 X REC 98.5 03/26/96 2307 CC8 9603057 -0,00019 03!26!96 2324 ISB 9602297 0.40760 0.5000 X REC 81.5 03/26196 2355 CCV 9602167 4.98968 5.0 X REC 99.8 03/26!96 2359 GCB 9603057 -0,00000 03(27196 0010 Method......: EPA 200.7 Batch .............: 7412 Analyst,..: gef~ Description.: Metals Analyst s(ICAP), Trace Detection Limit.-.: 0.04 Parameter...: Nickel (Ni) Units .............: mg/L OC Lab ID M Reagent OC Result True Yalue Orig. Value Alt. Value Calculation Result Analyzed ICV 9603122 1.91973 2.00 X REC 96.0 03!26196 1856 IC8 9603057 -0.00007 03/26/46 1942 ISB 9602297 0,85652 1.00 X REC 85.7 03/26/96 2008 CCY 9602167 2,42056 2.5 X REC 96.8 03/26/96 2047 cC8 9603057 0,00053 03/26/96 2103 CCV 9602167 2,44219 2.5 X REC 97.7 03/26/96 2154 CCB 9603057 0,00110 03!26/96 2209 MD 960720-2 D 0,00136 0.00090 ABS Diff. 0.00046 03/26/96 2216 PDS 960720-2 D 960228X 0,83047 1-000 0.00090 X REC 83.0 03)26!96 2224 CCV 9602167 2.45846 2.5 X REC 98.3 03/26/96 2307 CCB 9603057 0.00072 0326!46 2324 ISB 9602297 0.82648 1.00 X REC 82.6 0326/46 2355 CCV 9602167 2.49867 2.5 X REC 99.9 03/26/96 2359 CC8 9603057 0.00289 03/27/96 0010 Method.....,: EPA 200.7 Batch ............ .: 7412 analyst...: gef Description.: Metals Ana lysi s(lC0.P), Trace Detection Limit.. ,: 0.01 Parameter..,: Silver (Ag) Units ............ .: mg/L OC lab ID M Reagent OC Result true Value Orig. Value Alt. Value Calculation Result Anelyxed tCV 951024P 1.96639 2.00 X REC 98.3 03/26/96 1907 ICB 9603057 -0.00045 03/26/96 1942 ISB 4602297 0.95751 1.000 X REC 95.8 03/26/96 2008 cCV 951113E 2.54244 2.500 X REC 107.7 03/26/96 2059 CC8 9603057 -0.00055 03/26/96 2103 CCV 951113E 2.53695 2.500 X REC 101.5 03/26!96 2158 CCB 9603057 -0.00222 0326!96 2209 MD 960720-2 D •0.00306 -0.00386 ABS Diff. 0.00080 03/26/96 2216 PDS 960720-2 D 960228X 0.91085 1.000 -0.00386 % REC 91.5 03/26/96 2224 Page 31 ..,.~~,..~•m. o..~.~..a m. ~., w.~ ~..~ m..~......,.o.o.....,e...w.a.A.e.a.,.A..e.,,...~,:..,...~. wee. ~.,.>~~.o.>~,.e.~e .,, a. w. m.> m.. ~.~..,~.... o..<.. m.~.e. ~.., ~.a gyn. ~> ~ ~...,. ~.e,..~e,. ~ ~.~.eo swam ~ a s. m...w.. ~.ma. a co. ~.,..