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CORE LABORATORIES D U A L I T Y C O N T R O L R E P O R T Job Nunfxr; 960720 Report Date: 04/02/96 CUSTOMER: Greys tone PROJECT: ATTN: Jeff Spinzig Method...,..: EPA 204-2 Batch .............: 7377 AnalYSt...: lmt~ Description.: Antimony (GFAA) Detection Limit...: 0.005 Parameter...: Antimony (Sb) Units .............: mg/L OC Lab ID M Reagent DC Result True Value Orig. Value Alt. Value Calculation Result Analyzed CCB 03256 0,00078 0385/96 1256 MB 0320 -0.00005 03/25/96 1318 LCS 980214) 0.04358 0.040000 Y. REC 109.0 03/25/96 1325 MS 960701-1 T 9510160 0.02307 0.020000 0.00638 X REC 83.5 03/25/96 1340 MSD 960701-1 T 9510160 0.02419 0.020000 0.00638 0.02307 X REC 89.0 03125/96 1348 RPD 4.7 MD 960701-1 7 0.00924 0.00638 ABS Diff. 0.00286 03/25/96 1355 SD 960701-1 T 0.00117 0.00638 X Diff. 03/25/96 1403 CCV 9603140 0.04852 0.0500 X REC 97.0 03/25/96 1420 CCB 03256 0.00100 03/25196 1427 MD 960720-1 D -0.00076 0.00067 ABS Diff. 0.00143 03/25/96 1439 PDS 960720-2 D 9602030 0.02318 0,020000 0,00076 X REC 112.1 03/25/96 1446 SD 960720.3 D -0.00120 -0.00040 X Diff. 03/25/96 1454 CCY 9603140 0.04702 0.0500 X REC 94.0 03/25/96 1501 CCB 03256 -0.00044 03/25/96 1505 Method......: EPA 239.2 Batch ............. : 7381 Analyst...: Lmt Description.: Lead (GFAA) Oetecticn Limit-.. : 0.002 Parameter,..: Lead (Pb) Units ............. : mg/L OC Lab ID M Reagent OC Result True Value Orig. Value Alt. Value Calculation Result Analyzed ICV 9603018 0.04176 0,0400 Y. REC 104.4 03125!96 1613 ICB 03256 -0.00030 03/25/96 1619 MD 960720-1 D -0.00046 -0.00008 ABS Diff. 0,00038 03/25/96 1636 PDS 960720-2 D 9511'190 0.01961 0.020000 0.00036 X REC 96.2 03/25/96 1643 SD 960720-3 D 0.00027 0.00010 X Diff- 03(25/96 1649 ccV 9603010 0.05089 0.050 X REC 101.8 03!25/96 1657 CCB 03256 -0.00043 03/25/96 1704 CCV 9603010 0.05380 0.050 X REC 107.6 03/25/96 1815 CCB 03256 -0.00014 03/25/96 1822 CCV 9603010 0.05448 0.050 X REC 109.0 03!25196 1926 CCB 03256 0,00065 03/25/96 1933 Method,-....: EPA 200.7 Batch ..... ........: 7412 Analyst...: gef Description.: Metals Ana lysis([CAP ), Trace Detection Limit...: 0.05 Parameter...: Arsenic (AS) Units .............: mg/L DC Lab ID M Reagent OC Result True Value Orig, Value Alt, Value Calculation Result Anel yzed ICV 9603122 2.05384 2.00 X REC 102.7 03/26/46 1856 ICB 9603057 0.00361 03/26/96 1942 (SB 9602297 0.92497 1.00 X REC 92.5 03/26/96 2008 CCV 9602167 2.55879 2.5 X REC 102.4 03/26/96 2047 CCB 9603057 -0.00171 03/26/96 2103 CCV 9602167 2.60363 2.8 X REC 104,1 03/26/96 2154 CCB 9603057 -0.00093 03/26/96 2209 MD 960720-2 D 0.0027/ 0.00152 ABS Diff. 0.00125 03/26/96 2216 PDS 960720-2 D 960228% 0.92005 1.000 0.00152 X REC 41.9 03/26{96 2224 CCV 9602167 2.55641 2.5 X REC 102,3 03/26(46 2307 CCB 9603057 0.00214 03/26/96 2324 Page 27 .~>i~PVn~u~uO~.gCe.lav~n~Ca~um~v~~vw.rnm r.~v4~gV~nN ~.O~snoe O~n.~'ov^~VMeMV~w~ P.omevT V¢~¢~~e~v vJ~O~q ~T d. it M v asV ~~ >a~M1 ~ vYO n v/im~ ~P Ion ua ima• uuo ~v~a yam V ~+~~ ~~ev.~ ~m got N ra w romm n.p v n tom. Tv F ~ 00~ /b.IYq