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i <br />CORE LABORATORIES <br />D U A L I T Y C O N T R O L R E P O R T <br />Job Nunber: 960720 Report Oate: 04(02!46 <br />CUSTOMER: Greystone PROJECT: ATTN: Jetf Spinzig <br />Method......: EPA 353.2 Batch .............: 7263 Analyst...: dme~ <br />Description.; Nitrogen, N02, N03 (Auto Ld Red.) Detection Limit...: 0.01 <br />Parameter...: Nitrogen, Nitrite as N (N02-N) Unfits .............: mg/L <br />OC Lab ID M Reagent <br />ICL G951027A <br />ICB <br />CCB <br />CCV G950330A <br />MD 960718-4 U <br />MS 960718-4 U G950330A <br />MSD 960718-4 U G950330A <br />LCS G951027A <br />CCB <br />CCV G950330A <br />MD 960720-4 F <br />MS 960720-4 F G950330A <br />CCB <br />CCV G950330A <br />0C Result Dil. Value Orig. Value Alt. Value Calculation Result <br />0.97 1.000000 X REC 97.0 <br />0.00 <br />0.00 <br />2.08 2.000000 Y. REC 104.0 <br />0.00 0.00 A8S Diff- 0 <br />1.03 1.000000 0.00 X REC 103.0 <br />1.01 1.000000 0.00 1.03 Y. REC 101.0 <br /> RPD 2.0 <br />1.03 1.000000 X REC 103.0 <br />0.00 <br />2.09 2.000000 X REC 104.5 <br />0.00 0.00 ABS Diff. 0 <br />1.07 1.000000 0.00 X REC 107.0 <br />0.00 <br />2.01 2.000000 X REC 100.5 <br />Analyzed <br />03!21!96 0810 <br />03/21/96 0905 <br />03/21/96 0910 <br />03/21/96 0915 <br />03/21/96 0930 <br />03!21146 0935 <br />03/21/96 1010 <br />03/21/96 1020 <br />03121/96 1025 <br />03!21/96 1045 <br />03/21/96 1055 <br />03/21/96 1125 <br />03!21/96 1130 <br />Method...... : 600/8-78-017 MF Batch .............: 7269 Analyst...: dme <br />Description. : Coliform Bacteria Analysis Oeteciion Limi [-..: 1 <br />Parameter...: Coliform, Total Units .............: CFU/100 mL <br />OC Lab ID M Reagem DC Result True Value Orig. Value Al [. Value Calculation Result Analyzed <br />M8 0 03/20/96 1130 <br />MD 960720-1 U 0 0 ABS Diff. D 03!20!96 1130 <br />Method......: EPA 245.1 Batch .............: 7271 Analyst...: lmt <br />Description,: Mercury (CVAA) Detection Limit...: 0.0002 <br />Parameter...: Mercury (Ng) Units .............: mg/L <br />DC Lab 10 M ReagenC DC Result Dil. Value Orig. Ya lue Alt. Value Catcul ati on Result Analyzed <br />ICV 9602276 0.00362 0.004000 X REC 40.5 03!22/96 0900 <br />IL8 03216 O.000OB 03!22!96 0902 <br />M8 032167 -0,00008 03/22/96 0903 <br />MB 032160 -0.00010 03/22/96 0905 <br />MS 960647-4 T 960321H 0.00534 0.005000 0.00005 X REC 105.8 03/22/96 0908 <br />MSD 960647-5 T 960321H 0.00484 0.005000 0.00005 0.00534 X REC 95.8 03!22!96 0909 <br /> RPD 9.8 <br />MS 960647-10 T 960321H 0.00509 0.005000 -0.00001 X REC 102.0 03/22/96 0912 <br />MSD 960647-11 T 960321H 0.00462 0.005000 -0.00001 0,00509 X REC 92.6 03/22/96 0914 <br /> RPD 9.7 <br />CCV 9602274 0.00375 0.004000 X REC 93.8 03!22!46 0919 <br />CCB 03216 0.00005 03/22/96 0920 <br />MD 960711-1 7 0,00005 0.00005 ABS Diff. 0.00000 03/22/96 0922 <br />MS 960732-1 T 9b0321H 0.00490 0.005000 0.00008 X REC 96.4 03!22/96 0925 <br />MS 960681-2 T 960321H 0.00462 0.005000 -0.00007 X REC 92.6 03122!96 0934 <br />MSD 960681-2 T 960321H 0.00484 0.005000 -0.00001 0.00462 X REC 97.0 03!22!96 0936 <br /> RPD 4.7 <br />CCV 9602274 0.00428 0.004000 % REC 107.0 03/22/96 0947 <br />CCB 03216 0,00005 03!22!96 0942 <br />MS 960701-1 T 960321H 0.00474 0.005000 0.00036 X REC 87.6 03!22!46 0944 <br />Page 24 <br />Mi m~.TYO.q nVCV.Wnuwfq.l~b.mw rcw~.~murN.n~nvrp~m~.meen~.Ynnw w.mWUav~. r~yumm.OmCM.O~u+~a~sVMS~p <br />~e a. pa. m/u T. ~~. v¢~F. ~ v Mvn mrt0i ~.ne~,.a rV V~ ~ ~ o ri ~v/~ b I~ nP .ne~.~. fly nte'~ MM Y rV WaS. n M v n M. Nom/ O~wTw .tPe~ YCe, ld~va <br />