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LABORATORY CONTROL SAMPLE SVALDATION REPORT General Chemistry Lot-Sample #...: D4D090366 Matrix.........: WATER PERCENT RECOVERY RPD PREPARATION- PREP PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE BATCH # pH WO#:GEEFRIAA-LCS/GEEFRIAC-LCSD LCS Lot-Sample#: D4D1 10000-096 100 (97 - 102) MCAWW 150.1 04/10/04 4102096 100 (97 - 102) 0.14 (0-5.0) MCAWW 150.1 04/10/04 4102096 Dilution Factor: 1 Analysis Time.. ; 23:14 Ammonia as N WO#:GDSVOlAC-LCS/GDSVO lAD-LCSD LCS Lot-Sample#: D4D1 40000-426 107 (90 - 110) MCAWW 350.1 04/14/04 4105426 105 (90 - 110) 2.4 (0-10) MCAWW 350.1 04/14/04 4105426 nilution Factor: 1 Analysis Time.. ; 01:00 Fluoride WO#:GEOCGIAC-LCS/GEOCGIAD-LCSD LCS Lot-Sample#: D4D2 60000-413 96 (87 - 114) SM18 4500-F C 04/26/04 4117413 99 (87 - 114) 2.5 (0-16) SM18 4500-F C 04/26/04 4117413 Dilution Factor: 1 Analysis Time.. : 11:30 Nitrate WO#:GD5881AC-LCS/GD5881AD-LCSD LCS Lot-Sample#: D4D1 40000-541 93 ~ (86 - 110) MCAWW 353.2 04/10/04 4105541 92 (86 - 110) 0.86 (0-10) MCAWW 353.2 04/10/04 4105541 Dilution Factor: 1 Analysis Time.. : 17:45 Nitrate-Nitrite WO#:GD53L1AC-LCS/GD53L1AD-LCSD LCS Lot-Sample#: D4D1 400C0-497 101 (90 - 110) MCAWW 353.2 04/14/04 4105497 99 (90 - 110) 2.4 (0-10) MCAWW 353.2 04/14/04 4105497 Dilution Factor: 1 Analysis Time.. : 01:00 Nitrite WO#:GEEFElAC-LCS/GEEFEIAD-LCSD LCS Lot-Sample#: D4D1 10000-099 93 (86 - 110) MCAWW 353.2 04/10/04 4102099 92 (86 - 110) 0.66 (0-10) MCAWW 353.2 04/10/04 4102099 Dilution Factor: 1 Analysis Time.. ; 17:45 Specific Conductance WO#:GD8H21AC-LCS/GDSH2IAD-LCSD LCS Lot-Sample#: D4D1 40000-609 102 (S9 - 209) MCAWW 120.1 04/14/04 4105608 99 (89 - 109) 3.4 (0-7.0) MCAWW 120.1 04/14/04 4105608 Dilution Pact or: 1 Analysis Time.. : 17:50 Sulfate WO#:GEDA9IAC-LCS/GEDA9IAD-LCSD LCS Lot-Sample#: D4D1 60000-635 110 (89 - 113) MCAWW 375.4 04/16/04 4107635 109 (89 - 113) 0.85 (0-15) MCAWW 375.4 04/16/04 4107635 Dilution Factor: 1 Analysis Time.. ; 11:00 (Continued on next page) 31