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u CORE LABORATORIES L A B O R A T O R Y T E S T R E S U L T S Job Nunber: 972391 Date: 09130/97 CUSTOMER: Greystone ~ ~ ~ PROJECT: COSTILLA ATTN: Nick Mathis Customer Saapte ID: MN-1 Laboratory Sample l0: 972341-1 Date Sampled......: 08128/97 Date Received.......: 08/28/97 Time Sampled......: 10:15 Time Received.......: 16:20 Sample Matrix.....: Wafer TEST METHOD PARAMETER/TEST DESCRIPTION SAMPLE RESULT REPORTING LIMIT UNITS DATE TECN EPA 239.2 Lead (Pb), Diss. <0.002 0.002 mg/L 09/09/97 lmt EPA 200.7 Manganese (Mn), Diss. <0.001 0.001 mg/L 09/10/97 ark EPA 245.1 Mercury (Hg), Diss. <0.0002 0.0002 ng/L 09/03!97 veb EPA 200.7 Nickel (Ni ), Diss. <0.005 0.005 mg1L 09/10/97 ark EPA 270.2 Selenium (Se), Diss. <0.005 0.005 mg/L 09105{97 lmt EPA 200.7 Silver (Ag), Diss. <0.005 0.005 mg/L 09110/97 ark EPA 279.2 Thalliun (Tl), Diss. <0.002 0.002 mg/L 09103/97 lmt EPA 200.7 Zinc (Zn), Diss. 0.007 0.005 mg/L 09(10!97 ark 54-846 35108 Extraction (Sep. Fume!) Herb. Separatory Fumel Liq/Liq Extraction Conplete 09/03/97 rMn EPA 608 Pesticides/PCBs (Organoch brine) Aldrin HD 0.004 ug/L 09/13/97 smc alphe-BHC ND 0.003 ug/L 09/13/97 smc beta-BNC ND 0.006 ug/L 09!13/97 smc delta-BHC ND 0.009 ug/L 09/13/97 smc gamma-BHC (Lindane) ND 0.004 ugfL 09/13/97 smc Chlordane ND 0.014 ug/L 09/13/97 smc 4,4'-DOD ND 0.011 ug/L 09/13/97 smc 4,4'-DDE ND 0.004 ug/L 09/13/97 smc 4,4~-DDT ND 0.012 ugfL 09/13!97 smc D ieldrin ND 0.002 ug/L 09/13/97 smc Endosulfan I ND 0.014 ug1L 09113147 smc Endosulfan II ND 0.004 ug/L 09/13/97 smc Endosulfan sulfate ND 0.066 ug/L 09113197 smc Erdrin ND 0.006 ug/L 09/13/97 smc Endrin aldehyde ND 0.023 ug/L 09!13/97 smc Heptachlor ND 0.003 ug/L 09/13/97 smc Heptachlor epoxide ND 0.083 ug/L 09/13/97 smc Toxaphene ND 0.24 ug/L 09/13/97 smc Aroclor 1016 ND 0.05 ug/L 09/10/97 smc Aroclor 1221 ND 0.05 ug/L 09/10/97 smc Aroclor 1232 ND 0.05 ug/L 09/10/97 smc Aroclor 1242 ND 0.05 ug/L 09/10/97 smc Aroclor 1248 ND 0.05 ug/L 09/10/97 smc Aroclor 1254 ND 0.05 ug/L 09/10/97 smc Aroclor 1260 ND 0.05 ug/L 09/10/97 smc EPA 608 Extraction (Sep. Fume!) Chlor. Pest Separatory Fumel Liq/Liq Extraction Complete 09102197 rwm Page 3 ep yr,MU nun, m~+a nuywµnccmawvi n iro rev. y,wn r~wn in~um,um /v ~rarwar ypy~ er n, nwri b nw,. ncu.nw ,w mngmy uf. inn Saar Nf o..n mu M uW~r¢u rn ui r,. wrngf w mrw un. rmi ,.p,f W pr,.wn rM1 Lwr µyrmr er Car, L~mnTC Cv~ lamnww. 'uw.w m.cn m •ur.nry w rp.nvv'en war n. a ~meW.01 ~+, rq, am nor„w ~MCVm fuN ~~ ro in. or m~rnvT. wiw evnmc w Oro rWwr er ury y pu. coYw o~v ~mwY. o~conv ti w yy ~ cwntbr ~rr'r rn'a uc rar n ~W v r,lq umn rs ury War wrgww Rw rp:n ,N mr 0~ r,prmrrc wl ~n ..ny w n cur +rRVr ~n~ ~r~nm mwu ar Car. acorn vn.