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MATRIB SPl]D3 aatMOrx BVALDATION REPORT <br />General Chemistry <br />Client Lot #...: D4A160373 Matrix.........: WATER <br />Date Sampled...: 01/16/04 09:01 Date Received..: 01/16/04 <br /> PERCHNT RECOVERY RPD PREPARATION- PREP <br />PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ~ ANALYSIS DATE BATCH # <br />Ammonia a9 N WO#: F75RLiDF-MS/F75RL1DG-MSD MS Lot-Sample #: D.4A160226-002 <br /> 93 (44 - 130) MCAWW 350.1 01/23/04 4027340 <br /> ~95 (44 - 130) 0.94 (0-30) MCAWW 350.1 01/23/04 4027340 <br /> Dilution Pactor: 1 <br /> Analysis Time..: 18:00 <br />Chloride WO#: F7PTL1A1-MS/F7PTL1A2-MSD MS Lot-Sample #: D4A080288-001 <br /> 105 (90 - 110) MCAWW 325.2 01/19/04 4020318 <br /> 103 (90 - 110) 1.7 (0-10) MCAWW 325.2 01/19/04 4020318 <br /> Dilutitm Pactor: 1 <br /> Analysis Time..: 16:00 <br />Fluoride WO#: F76TS1FA-MS/F76TS1FC-MSD MS Lot-Sample #: D4A160373-001 <br /> 97 (87 - 107) SM18 4500-F C 01/28/04 4028417 <br /> .96 (87 - 107) 0.41 (0-30) SM18 4500-F C 01/28/04 402841.7 <br /> Dilution Factor: 1 <br /> Analysis Time..: 12:00' <br />Nitrate-Nitrite WO#: F76JA1D9-MS/F76JAlEA-MSD MS Lot-Sample #: D4A160331-001 <br /> 92 (62 - 119) MCAWW 353.2 01/20/04 4021508 <br /> 92 (62 - 119) 0.10 (0-30) MCAWW 353.2 01/20/04 4021508 <br /> Dilution Pactor: 1 <br /> Analysis Time..: 14:00 <br />Nitrite WO#: F753V1C1-MS/F753V1C2-MSD MS Lot-Sample #: D4A150391-020 <br /> 84 (69 - 121) MCAWW 353.2 01/17/04 4018112 <br /> 81 (69 - 121) 2.7 (0-10) MCAWW 353.2 01/17/04 4018112 <br /> Dilution Factoz: 1 <br /> Analysis Time..: 16:30 ' <br />Sulfate WO#: F70E41C0-MS/F70E41C1-MSD MS Lot-Sample #: D4A140145-001 <br /> 102 I (56 - 129) MCAWW 375.4 01/21/04 4022194 <br /> 95 I (56 - 129) 4.7 (0-15) MCAWW 375.4 01/21/04 4022194 <br /> Dilution Pactoz: 1 <br /> Analysis Time..: 16:00 <br />Calculatioru arc performed befoce rountling to avoid mundrofl errors in calwlasetl resulm. <br />I Estima[ed raulc Result wnemtntion exceeds the nlibasion ange. <br />34 <br />