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LABORATORY CONTROL SAMPLE DATA REPORT <br />General Chemistry <br />t Lot-Sample #...: D4A160373 <br />Matrix.........: WATER <br /> SPIKE MEASIIRED PSRCNT PREPARATION- PREP <br />PARAMRTER AMOIINT AMOUNT DNITS RECVRY RPD METHOD ANALYSIS DATE BATCH # <br />' <br />px WO#:F8GWDIAA-LCS/FBGWDIAC-LCSD LCS Lot-Sample#: D4A18000 0-115 <br /> 7.00 .7.03 NO IIIIita 100 MCAWW 150.1 ~ 01/17/04 4018115 <br /> 7.00 7.03 No IInita 100 0.0 MCAWW 150.1 01/17-01/23/04 4018115 <br /> Dilution Factor: 1 Analyaie Time.. : 20:38 <br />Ammonia as N WO#:FBLRLIAC-LCS/P8LKLIAD-LCSD LCS Lot-Sample#: D4A270000-340 <br /> 4.00 3.96 mg/L 99 ~ MCAWW 350.1 01/23/04 4027340 <br /> 4.00 3.92 mg/L 98 1.1 MCAWW 350.1 01/23/04 4027340 <br /> Dilution Factoz: 1 Analysis Time.. : 18:00 <br />Fluoride WO#:F8N8D1AC-LCS/F8NBDIAD-LCSD LCS Lot-Sample#: D4A280000-417 <br />' 5.00 5.30 mg/L 106 SM18 4500-F C 01/28/04 4028417 <br /> 5.00 5.30 mg/L 106 0.0 3M18 4500-F C 01/28/04 4028417 <br /> Dilution Factor: 1 Analyais Time.. : 12:00 <br />' Nitrate WO#:F8 C111AC-LCS/F8C111AD-LCSD LCS Lot-Sample#: D4A210000-534 <br /> 0.0500 0.0460 mq/L 92 MCAWW 353.2 01/17/04 4021534 <br /> 0.0500 0.0467 mg/L 93 1.5 MCAWW 353.2 01/17/04 4021534 <br />' Dilution Factor: 1 Analysis Time.. : 16:30 <br />Nitrate-Nitrite WO#:F8CXEIAC-LCS/FBCXElAD-LCSD LCS Lot-Sample#: D4A210000-508 <br /> 4.00 3.91 mg/L 98 MCAWW 353.2 01/20/04 4021508 <br />' 4.00 3.99 mg/L 100 2.0 MCAWW 353.2 01/20/04 4021508 <br /> Dilution Factoz: 1 Analysis Time.. : 14:00 <br />' Nitrite WO#:F8PQ41AC-LCS/F8PQ41AD-LCSD LCS Lot-Sample#: D4A180000-113 <br /> 0.0500 0.0460 mg/L 92 MCAWW 353.2 01/17/04 4018113 <br /> 0.0500 0.0467 mg/L 93 1.5 MCAWW 353.2 01/17/04 4018113 <br /> Dilution Factor: 1 Analysis Time.. : 16:30 <br />' <br />Sulfate WO#:F8DCI LAC-LCS/F8DC11AD-LCSD LCS Lot-Sample#: D4A220000-193 <br /> 25.0 25.8 mg/L 103 MCAWW 375.4 01/21/04 4022193 <br /> 25.0 25.7 mg/L 103 0.52 MCAWW 375.4 01/21/04 4022193 <br />' Dilution Pactoz: 1 Analysis Time..: 16:00 <br />Total DiasOlved WO#:FSMDJIAC-LCS/F8MDJIAD-LCSD LCS Lot-Sample#: D4A220000-177 <br />' <br />Solids <br /> 500 476 mg/L ~ 95 MCAWW 160.1 01/21/04 4022177 <br /> 500 495 mg/L 99 3.9 MCAWW 160.1 01/21/04 4022177 <br />' Dilution Factor: 1 Analysis Time..: 14:00 <br />_ (Continued on next page) <br />30 <br />