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LABORATORY CONTROL SAMPLE BVALIIATIOR RBPOBT <br />General Chemistry <br />Lot-Sample ~...: D4A160373 Matrix.........: WATHR <br /> PSRCHNT RHCOVSRY RPD PREPARATION- PRHP <br />PARAMHTER RECOVHRY LIMITS RPD LIMITS METHOD ANALYSIS DATH BATCH # <br />' pH WO#:F8GWDIAA-LCS/FSGWDIAC-LCSD LCS Lot-Sample#: D4A180000-115 <br /> 100 (97 - 102) MCAWW 150.1 01/17/04 4018115 <br /> 100 (97 - 102) 0.0 (0-5.0) MCAWW 150.1 01/17-01/23/04 4018115 <br />t Dilution Pactor: 1 Analyais Time. .: 20:26 <br />Ammonia as N WO#:FBLIQ,lAC-LCS/F8LHI,lAD-LCSD- LCS Lot-Sample#: D4A270000-340 <br /> 99 f90 - 110) MCAWW 350.1 01/23/04 4027340 <br /> 98 (90 - 110) 1.1 (0-10) MCAWW 350.1 01/23/04 4027340 <br /> Dilution Pactor: 1 Analysis Time. .: 18:00 <br />Fluoride WO#:FBNBDIAC-LCS/F8N8D1AD-LCSD LCS Lot-Sample#: D4A280000-417 <br /> 106 (87 - 114) SM18 4500-F C 01/28/04 4028417 <br /> 106 (87 - 114) 0.0 (0-16) SM18 4500-F C 01/28/04 4028417 <br /> Dilution Pactor: 1 Analysis Tfine. .: 12:00 <br />' Nitrate WO#:F8C111AC-LCS/F8C 111AD-LCSD LCS Lot-Sample#: D4A210000-534 <br /> 92 (86 - 110) MCAWW 353.2 01/17/04 4021534 <br /> 93 (66 - 110) 1.5 (0-10) MCAWW 353.2 01/17/04 4021534 <br />' Dilution Pactor: 1 Analysis Time.. : 16:30 <br />Nitrate-Nitrite - WO#:F8CXEIAC-LCS/FBCXElAD-LCSD LCS Lot-Sample#: D4A210000-508 <br /> 98 (90 - 110) MCAWN 353.2 01/20/04 4021508 <br />' 100 (90 - 110) 2.0 (0-10) MCAWW 353.2 01/20/04 4021508 <br /> Dilution Pactor: 1 Analysis Tlme.. : 14:00 <br />Nitrite WO#:P8PQ41AC-LCS/FBPQ4IAD-LCSD LCS Lot-Sample#: D4A180000-113 <br />' 92 (86 - 110) MCAWW 353.2 01/17/04 4018113 <br /> 93 (86 - 110) 1.5 (0-10) MCAWW 353.2 01/17/04 4018113 <br /> Dilution Factor: 1 Analysis Time.. : 16:30 <br />' <br />Sulfate WO#:FSDCI3AC-LCS/FBDCIIAD-LCSD LCS Lot-Sample#: D4A220000-193 <br /> 103 - (89 - 113) MCAWW 375.4 01/21/04 4022193 <br /> 103 (89 - 113) 0.52 (0-15) MCAWW 375.4 01/21/04 4022193 <br /> Dilution Factor: 1 Analysis Time.. : 16:00 <br />Total Dissolved <br />' Solids <br />95 <br />99 <br />WO#:F8NIDJIAC-LCS/FBhIl)J1AD-LCSD LCS Lot-Sample#: D4A220000-177 <br />(86 - 106) MCAWW 160.1 01/21/04 4022177 <br />(86 - 106) 3.9 (0-20) MCAWW 160.1 01/21/04 4022177 <br />Dilution Factor: 1 Aaalysls Time..: 14:00 <br />(Continued on next page) <br />28 <br />