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MATRffi SPIKH SAMPLE DATA REPORT <br />TOTAI. Metals <br />Client Lot #...: D4A160373 Matrix.........: WATER <br />Date Sampled...: 01/16/04 15:42 Date Received..:01/16/04 <br />SAMPLE SPIRE MEASRD PERCNT PREPARATION- WORK <br />PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSES DATE ORDER # <br />Manganese <br />0.082 0.500 0.590 mg/L 102 MCAWW 200.7 01/21/04 F76TS1EQ <br />0.082 0.500 0.584 mg/L 101 1.0 MCAWW' 200.7 01/21/04 F76TS1ER <br /> Dilution Factor: 1 <br /> - Analysis Time..: 15:46 <br />Nickel <br />0.017 0.500 0.520 mg/L 101 MCAWW 200.7 01/21/04 F76TS1EV <br />0.017 0.500 0.516 mg/L 100 0.77 MCAWW 200.7 01/21/04 F76TS1EW <br /> Dilution Factor: 1 <br /> ' Analysis Time..: ,15:46 , <br />Potassium - <br />28 50.0 86.8 N mg/L 117 _ MCAWW 200.7 01/21-01/26/04 F76TS1EZ <br />28 50.0 86.6 N mg/L 117 0.30 MCAWW 200.7 01/21-01/26/04 F76TS1EM <br />- Dilution Factor: 1 <br /> Analysis Time..: 13:04 <br />Sodium <br />130 50.0 183 mg/L 104 <br />130 50.0 182 mq/L 103 <br />Dilution Factor: 1 <br />Analysis Time..: 13:52 <br />MCAWW 200.7 01/21-01/27/04 F76TS1ET <br />0.36 MCAWW 200.7 01/21-01/27/04 F76TS1EU <br />MS Lot-Sample #: D4A160373-001 Prep Batch #...: 4023505 <br />Antimony <br />0.00037 0.0400 0.0433 mg/L 107 MCAWW 200.8 01/26-01/27/04 F76TS1DV <br />0.00037 0.0400 0.0420 mg/L 104 3.2 MCAWW 200.8 01/26-01/27/04 F76TSiDW <br />Dilution Factor: 1 <br />Analysis Time..: 17:00 <br />ArBeniC <br />0.016 0.0400 0.0568 mg/L 103 MCAWW 200.8 01/26-01/27/04 F76TS1D3 <br />0.016 0.0400 0.0528 mg/L 93 7.3 MCAWW 200.8 01/26-01/27/04 F76TS1D4 <br />' Dilution Pactor: 1 <br />Analysis Time..: 17:00 <br />Barium <br />0.028 0.0400 0.0665 mg/L ~ 97 MCAWW 200.8 01/26-01/27/04 F76TS1D5 <br />0.028 0.0400 0.0640 mg/L 91 3.8 MCAWW 200.8 01/26-01/27/04 F76TS1D6 <br />Dilution Factor: 1 <br />Analysis Time..: 17:00 <br />(Continued on next page) <br />24 <br />