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<br />
<br />
<br />CORE LABORATORIES
<br />Q U A L I T Y C O N T R O L R E S U L T S
<br />Job Number: 962453 Date: 09/28/96
<br />CUSTOMER: Greys[one PROJECT: 484-03 ATTN: Ray Faciski
<br />Tes[ Method........: EPA 200.9 Batch .............: 13389 Analyst...: lmt
<br />Method Description.: Antimony (G FAA) Reporting Limit...: 0.002
<br />Parameter..........: Antimony (Sb) Units .............: mg/L
<br />OL Lab ID Reagent OC Result OC Result True Value Orig. Value Lalc. Result Units Date/Time
<br />CCB 09186 0.00049 09/18/96 1404
<br />Test Method........: EPA 420.1 Batch .............: 13516 Analyse...: dme
<br />Method Description.: Phenols, To[al Recoverable Reporting Limit...: 0.05
<br />Parameter..........: Phenol, Total Recoverable Units .............: mg/L
<br />OC Lab ID Reagent OC Result OC Resul[ True Value Orig. Value Calc. Result Units Date/Time
<br />ICL 960067 0.05 0.05 100.0 X REC 09/20/96 0924
<br />ILB 0.00 09/20/96 0924
<br />MB 0.00 09/20/96 0924
<br />MD 962453-1 0.00 0.00 0 ABS Diff. 09/20/96 0924
<br />MS 962453-1 G951008A 0.23 0.250000 0.00 92.0 % REL 09/20/96 0924
<br />CCV G951008A 0.50 0.500000 100.0 X REC 09/20/96 0924
<br />CCB 0.00 09/20/96 0924
<br />LLV G981005A 0.49 0.500000 98.0 % REC 09/20/96 0924
<br />C[8 0.00 09/20/96 0924
<br />LCS 960067 0.05 0.05 100.0 % REL 09(20(96 0924
<br />MB 0.00 09/20/96 0924
<br />CCV G951005A 0.50 0.500000 100.0 Y. REC 09/20/96 0924
<br />CCB 0.00 09/20/96 0924
<br />Test Method........: EPA 375.2 Batch ............. : 13522 Analyst...: dme
<br />Method Description.: Sulfate (Automated MTB, AAII) Reporting Limit... : 10.
<br />Parameter..........: Sulfate (504) Units ............ .: mgJL
<br />OC Lab ID Reagent OC Result
<br />ICL G960209q 52.40581
<br />ICB -0.28678
<br />CCV G960415E 78.19361
<br />CCB 0.03533
<br />LCS G960209A 49.25899
<br />CCV G960415E 79.97335
<br />CCB 0.03533
<br />MD 962377-52 31.75985
<br />MS 962377-52 G960610A 76.23241
<br />CCV G960415E 77.30262
<br />CLB 0.14261
<br />MD 962377-43 25.42812
<br />MS 962377-43 G960610A 73.28320
<br />LCS G960209A 48.14381
<br />C[V G960415E 78.37172
<br />CLB 0.03533
<br />MD 962377-15 21.17588
<br />MS 962377-15 G960610A 67.62521
<br />CCV G960415E 78.81686
<br />CCB 0.14261
<br />LLV G960415E 80.15117
<br />CCB 0.03533
<br />LCS G960209A 50.00110
<br />OC Result True Value Orig. Value Calc. Result Units Date/Time
<br />50.0 104.8 X REC 09/21/96 1332
<br /> 09/21/96 1334
<br />80 97.7 X REC 09/21/96 1401
<br /> 09/21/96 1403
<br />50.0 98.5 X REC 09/21/96 1426
<br />80 100.0 Y. REC 09/21/96 1430
<br /> 09/21/96 1432
<br /> 32.43535 0.67550 ABS Diff. 09/21/96 1439
<br />50.000000 32.43535 87.6 % REL 09/21/96 1441
<br />80 96.6 % REL 09/21/96 1500
<br /> 09/21/96 1502
<br /> 28.36412 2.43600 A8S Diff. 09/21/96 1509
<br />50.000000 28.36412 89.8 % REC 09/21/96 1511
<br />50.0 96.3 % REL 09/21/96 1524
<br />80 98.0 % REL 09/21/96 1529
<br /> 09/21/96 1531
<br /> 18.77849 2.39739 ABS Diff. 09/21/96 1551
<br />50.000000 18.77849 97.7 Y. REC 09/21/96 1554
<br />80 98.5 Y. REC 09/21/96 1558
<br /> 09/21/98 1800
<br />80 100.2 Y. REC 09/21/96 1625
<br /> 09/21/96 1627
<br />50.0 100.0 % REC 09/21/96 1632
<br />Page 19
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