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<br />CORE LABORATORIES
<br />O U g L I T Y C O N T R O L R E S U L T S
<br />Job Ninnber: 962453 Date: 09/28/96
<br />CUSTOMER: Greystone PROJECT: 484-03 ATTN: Ray Faciski
<br />Test Method........: EPA 245.1 Batch .............: 13301 Analyst...: lmt
<br />Method Description.: Mercury (CVAA) Reporting limit...: 0.0002
<br />Parameter..........: Mercury (Ng) Units .............: mg/L
<br />oC Lab ID Reagent OC Result OC Result True Value Orig. Value Calc. Result Units Date/Time
<br />CCV 950929N 0.005016 0.005000 100.3 X REC 09/17/96 1100
<br />CCB 09176 0.000085 09/17/96 1102
<br />MB 0916 0.000085 09/17/96 1107
<br />EB 1320 0.000085 09117196 1108
<br />SB 950929N 0.005288 0.005000 105.8 X REL 09/17/96 1110
<br />ED 962377-24 0.000085 0.000085 0.00000 ABS Diff. 09/17/96 1117
<br />CLV 950929N 0.005333 0.005000 106.7 7. REC 09/17/96 1120
<br />CCB 09176 0.000085 09/17/96 1122
<br />MD 962377-44 0.000085 0.000085 0.00000 ABS Diff. 09/17/96 1123
<br />MS 962377-54 950929N 0.005061 0.005000 0.000085 99.5 Y. REL 09/17/96 1128
<br />EB 1320 0.000085 09/17/96 1130
<br />58 950929N 0.005197 0.005000 103.9 % REL 09/17/96 1132
<br />ED 962377-25 0.000085 0.000085 0.00000 ABS Diff. 09/17/96 1138
<br />CLV 950929N 0.004835 0.005000 96.7 Y. REC 09/17/96 1140
<br />LCB 09176 0.000085 09/17/96 1142
<br />MD 962377-45 0.000085 0.000085 0.00000 ABS Diff. 09/17/96 1147
<br />MS 962377-55 950929N 0.004971 0.005000 0.000085 97.7 X REL 09/17/96 1150
<br />CLV 950929N 0.005152 0.005000 103.0 X REC 09/17/96 1158
<br />LCB 09176 0.000085 09/17/96 1200
<br />Test Method........: EPA 325.2 Batch ............. : 13304 Analyst...: sgm
<br />Method Description.: Chloride (Colon metric, AA II) Reporting Limit... : 0.5
<br />Parameter..........: Chloride Uni[s ............. : mg/L
<br />OC Lab ID Reagen[ OL Result OC Result True Value
<br />ICL G960116A 50.83659 50.0
<br />LCS G9601168 9.09986 10.0
<br />ICB 0.39646
<br />LCV G960506E 80.97899 80.0
<br />CCB 0.39646
<br />MD 962453-1 2.62992
<br />MS 962453-1 G960506A 53.63047 50.000000
<br />LCS G960116A 51.43637 50.0
<br />LLV G960506E 84.76120 80.0
<br />CCB 0.39646
<br />MD 962455-9 0.71320
<br />MS 962455-9 G960506A 51.10902 50.000000
<br />LLV G960506E 84.16977 80.0
<br />LLB 0.39646
<br />MD 962455-8 0.59433
<br />MS 962455-8 G960506A 52.75039 50.000000
<br />LCS G960116A 51.76418 50.0
<br />CCV G960506E 83.57847 80.0
<br />LLB 0.39646
<br />ED 962376-4 2.97295
<br />MD 962494-1 2.46912
<br />MS 962494-1 G960506A 54.34789 50.000000
<br />EB 0.39646
<br />CCV G960506E 81.33320 80.0
<br />CLB 0.39646
<br />ED 962377-22 0.39646
<br />Page 17
<br />Orig. Value Calc. Result Units Date/Time
<br /> 101.7 % REL 09/17/96 0930
<br /> 91.0 % REC 09/17/96 0930
<br /> 09/17/96 0930
<br /> 101.2 X REC 09/17/96 0930
<br /> 09/17/96 0930
<br />2.54949 3.1 RPD 09/17/96 0930
<br />2.54949 102.2 Y. REC 09/17/96 0930
<br /> 102.9 X REC 09/17/96 0930
<br /> 106.0 X REC 09/17/96 0930
<br /> 09/17/96 0930
<br />0.75285 0.03965 ABS Diff. 09/17/96 0930
<br />0.75285 100.7 Y. REC 09/17/96 0930
<br /> 105.2 % REC 09/17/96 0930
<br /> 09/17/96 0930
<br />0.71320 0.11887 ABS Diff. 09117)96 0930
<br />0.71320 104.1 X REC 09/17/96 0930
<br /> 103.5 Y. REC 09/17/96 0930
<br /> 104.5 Y. REC 09/17/96 0930
<br /> 09/17/96 0930
<br />2.83218 4.8 RPD 09/17/96 0930
<br />2.34865 0.12047 ABS Diff. 09/17/96 0930
<br />2.34865 104.0 % REC 09/17/96 0930
<br /> 09/17/96 0930
<br /> 101.7 X REL 09/17/96 0930
<br /> 09/17/96 0930
<br />0.39646 0.00000 ABS Diff. 09/17/96 0930
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