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IC~E~I CORE LABORATORIES D U A L I T Y C O N T R O L R E S U L T S Job Number: 962453 Date: 09/28/96 CUSTOMER: Greys tone PROJECT: 484-03 ATTN: Ray Faciski Test Method........: EPA 200.9 Batch .............: 13088 Analyst...: lmt Method Description.: Selenium (G FAA) Reporting Limit...: 0.005 Parameter..........: Selenium (Se) Units .............: mg/L OL Lab ID Reagent OC Result OC Resul[ True Value Orig. Value Calc. Result Units Date/Time LCV LCB 960722C 09106 0.05151 0.00045 0.050 103.0 X REC 09/10/96 1920 09/10/96 1924 Test Method........: EPA 160.1 Batch ............. : 13117 Analyst...: sgm Method Description.: Solids, Total Dissolved (TDS) Reporting Limit... : 10 Parameter..........: Solids, Total Dissolved (TOS) Units ............. : mg/L OC Lab ID Reagent OL Result OL Result True Value Orig. Value Calc. Result Units Date/Time MB 0 09/10/96 1755 LCS G960724A 506 500 101.2 % REC 09/10/96 1755 EB 0 09/10/96 1755 ED 962377-23 50 50 0 ABS Diff. 09/10/96 1755 MD 962453-1 188 188 0.0 RPD 09/10/96 1755 Test Method........: EPA 200.9 Batch ..... ........: 13251 Analyst...: lmt McThod Description.: Lead (G FAA) Reporting Limit...: 0.002 Parameter..........: Lead (Pb) Units ..... ........: mg/L 0C Lab ID Reagent OC Result ICV 9607228 0.04176 ICB 09156 -0.00075 CCV 960722C 0.04994 CCB 04156 -0.00063 CCV 960722C 0.04916 CCB 09156 -0.00087 MB 0913 -0.00026 LCS 960097 0.03987 MS 962421-1 960624E 0.05595 MD 962421-1 0.03737 MB 0911 -0.00043 LCS 960829H 0.03752 MD 962446-1 0.00005 CCV 960722C 0.04982 CCB 09156 -0.00055 MS 962446-2 960624E 0.02403 CLV 960722C 0.04969 CCB 09156 0.00052 MB 0911 -0.00145 LCS 960829H 0.03992 SD 962446-11 -0.00058 MD 962446-15 0.00100 CLV 960722C 0.05010 LLB 09156 -0.00072 MS 962446-16 960624E 0.02395 CCV 960722C 0.04989 CCB 09156 -0.00181 SD 962447-2 0.00173 MD 962453-1 -0.00037 PDS 962453-2 960912H 0.02070 OC Result True Value Orig. Value Calc. Result Units Date/Time 0.0400 104.4 % REL 09/15/96 1407 09/15/96 1413 0.050 99.9 X REC 09/15/96 1525 09115196 1531 0.050 98.3 % REC 09/15/96 1648 09/15/96 1655 09/15/96 1711 0.053500 74.5 % REC 09/15/96 1714 0.020000 0.03721 93.7 % REC 09/15/96 1721 0.03721 0.4 RPD 09/15/96 1724 09/15/96 1727 0.040000 93.8 % REC 09/15/96 1731 0.00183 0.00178 ABS Diff. 09/15/96 1737 0.050 99.6 Y. REC 09/15/96 1744 09/15/96 1747 0.020000 0.00380 101.2 X REC 09/15/96 1751 0.050 99.4 % REC 09/15/96 1821 09/15/96 1824 09!15!96 1832 0.040000 99.8 X REC 09/15/96 1835 0.00048 Y. Diff. 09/15/96 1842 0.00095 0.00005 ABS Diff. 09/15/96 1858 0.050 100.2 % REC 09/15/96 1905 09/15/96 1909 0.020000 0.00218 108.8 % REC 09/15/96 1912 0.050 99.8 % REC 09/15/96 1945 09/15/96 1948 0.01174 % Diff. 09/15/96 1958 -0.00080 0.00043 ABS Diff. 09/15/96 2005 0.020000 -0.00048 105.9 X REC 09/15/96 2012 Page 15 M wM~rn ~n~n.. oo nen. m ~n~v.pwai n~a Boni enq in .na Fo e+oe •ea ~mn ~nro~myio~ ago m+~n~e .uoo~~u q ne •~~em q. nmy..cWUw eno [o~vpenuei u.. m. rry~o r n,a oan m.a. M wv~¢er ~nwia w~~~om or ~ni,rorn~ ia~s uor.uw rao~ew.i inn ceai iw.] s ~ a1 Cpn •em~e~em~ Cc~u un~~a ~o~mr ~owa.w mnn np ~.p.. ~nrv a ~wr.rni n~en..~o aaa .n ~..oi~~~ a an. Ma nn ..mn~.rv a~x ivm. ume a ~e ~ e o main r, pees eoe~e4w or mciu men.y e~ a.. o-i pss w.i o~ one m.nwi veo.nv wn e. yno in .o~~cr.o~ ~m an. ~, .ucn r.m~ n ~aeE m M~+een ie v.y .ns ~raua.nr Tn..wn anyi nc~ o. r.pm~w .~...pe a~ n e.n..ninyi ~~. +~~nT ewrwu m Cye l~m~eiem