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• Table 6-8 <br />Parameter, Procedure and Reference List for Phase II Sampling at <br />Nuclarline <br />November, 1986 <br />Parameter Procedure <br />Sample Preparation Samples were dried at 30-35°C. Samples <br />were crushed to pass a 10-mesh sieve <br />(excessive grinding was avoided). <br />Subsampling less than U.S.D.A. Handbook 60, 1969 - Diagnosis and <br />2 mm fraction Improvement of Saline and Alkali Soils, <br />Method 1, pp. 83-84. <br />1. Preparation of saturation U.S.D.A. Handbook 60,i1ethods 2 and 3a, <br /> extract and saturation pp. 84 and 88, and idethod 27b, p. 101. <br /> percentage determination 10-mesh sieve. <br />2, pH (determination using U.S.D.A. Handbook 60, Method 21a, p. 102. <br /> saturated paste 10-mesh sieve. <br />3. Conductivity of saturation Sandoval and Power, U.S.D,A, Handbook 525, <br /> extract in mmhes/cm 1977, Laboratory Methods Recommended for <br /> at 25°C. Chemical Analysis of Mined Land Spoils and <br /> Overburden in ~.Jestern Unitetl States, Method 1, <br /> pp. 22-24. 10-mesh sieve. <br />4. Total Sulfur EPA, 1978; Field and Laboratory Methods <br /> Applicable to Overburden and Minesoil, <br /> EPA-600/2-78- 054, pp. 51-55. 60-mesh sieve. <br />5. Sulfur Fractionation AST;d, 1980, Gaseous Fuels - Coal and Coke - <br /> Atmospheric Analysis - Annual Book of ASTM <br /> Standards, Part 26. 60 mesh sieve. <br />6. Neutralization Potential USDA Handbook 60, Method 23C, p. 105, 60 mash <br />sieve. <br />7. Acid Base Potential Smith et al., 1974. Mine Spoil Potentials for <br />Soil and Water Quality, EPA-670/2-74-070, <br />pp. 48-49. 60 mesh sieve. <br />8. Manganese Methods of Soil Analysis, 1982. Part 2 - <br />Chemical and Microbiological Properties, <br />Method. 18-3,4, pp, 319-320. 10 mesh sieve, <br />. 9. Nickel, Zinc Methods of Soil Analysis, 1982. Part 2 - <br />Chemical and ticrobiological Properties, <br />Method 19-3.3, pp, 331-333. 10 mesh sieve. <br />6-40 Revised 11/01/86 <br />