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ACZ <br />Laboratories, <br />Batch A distinct set of samples analyzed at a specifc time <br />Found Value of the DC Type of interest <br />Limit Upper limit for RPD, in %. <br />Lower Lower Recevery Limit, in % (except for LCSS, mg/Kg) <br />MDL Method Detection Limit. Same as Minimum Reporting Limit. Allows for instrument antl annual fluctuations. <br />PCN/SCN A number assigned to reagents/standards to trace to the manufacturer's certificate of analysis <br />POL PraIXicel Quantitation Limit, typically 5 times the MDL. <br />OC True Value of the Control Sample or the amount added to the Spike <br />Rec Amount of the true value or spike added recovered, in % (except for LCSS, mg/Kg) <br />RPD Relative Percent Difference, calculation used for Duplicate OC Types <br />Upper Upper Recovery Limit, in % (except for LCSS, mg/Kg) <br />Sample Value of the Sample of interest <br />AS Analytical Spike (Post Digestion) LFM Laboratory Fortified Matdx <br />ASD Analytical Spike (Post Digestion) Duplicate LFMD Laboratory Fortified Matrix Duplicate <br />DUP Sample Duplicate LRB Laboratory Reagent Blank <br />LCSS Laboratory Control Sample • Soil MS/MSD Matriz Spike/Matrix Spike Duplicate <br />LCSW Laboratory Control Sample -Water PBS Prep Blank -Soil <br />LFB Laboratory Fortified Blank PBW Prep Blank -Water <br /> <br />Blanks Verifies that there is no or minimal contamination in the prep method procedure. <br />Control Samples Vedfies the accuracy of the method, inGuding the prep procedure. <br />Duplicates Vexes the precision of the instrument and/or method. <br />Spikes/Fortified Matrix Determines sample matdx interterences, if any. <br />B Analyte concentration detected at a value between MDL and PDL. <br />H Analysis exceeded method hold time. pH is a field test with an immediate hold time. <br />R Poor spike recovery accepted because the other spike in the set fell within the given limits. <br />T High Relative Percent Difference (RPD) accepted because sample concentrations are less than 10x the MDL. <br />U Analyte was analyzed for but not detected at the indicated MDL <br />V High blank data accepted because sample concentration is 10 times higher than blank concentration <br />W Poor recovery for Silver quality wntrol is accepted because Silver often precipitates with Chloride. <br />X Quality control sample is out of control. <br />Z Poor spike recovery is accepted because sample cencenUation is four times greater than spike concentration. <br />(1) EPA 60014-83-020. Methods for Chemical Analysis of Water and Wastes, March 1983. <br />(2) EPA 600/R-93-100. Methods for the Determination of Inorganic Substances in Environmental Samples, August 1993. <br />(3) EPA 600/R-94-111. Methods for the Determination of Metals in Environmental Samples -Supplement I, May 1994. <br />(5) EPA SW-846. Test Methods for Evaluating Solid Waste, Third Edition with Update III, December 1996. <br />(6) Standard Methods for the Examination of Water and Wastewater, 19th edition, 1995. <br />(1) OC results calculated from raw data. Results may vary slightly if the rounded values are used in the calculations. <br />(2) Soil, Sludge, and Plant matrtces for Inorganic analyses are reported on a dry weight basis. <br />(3) Animal matdces for Inorganic analyses are reported on an "as received" basis. <br />REPIN03.11.00.01 <br />L37592: Page 6 of 9 <br />