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ACZ Laboratories, Inc. <br />• 2773 Downhill Onve Steamboat Springs CO 80487 (800) 334 549. <br />Batch A distinct set of samples analyzed at a specific time <br />Found Value of the QC Type of interest <br />Limi( Upper limit for RPD, in %. <br />Lower Lower Recovery Limit, in % (ezcepi for LCSS, mg/Kg) <br />MDL Method Detection Limit. Same as Minimum Reporting Lirtet. Allows for instrument and annual fluctuations. <br />PCN/SCN A number assigned to reagents/standards to trace to the manufacturer's certifcate of analysis <br />PQL Practical Quantita[ion Limit, typically 5 times the MDL. ' <br />OC True Value of the Control Sample or the amount added to the Spike ~ <br />Rec Amounf of the true value or spike added recovered, in % (ezcepi for LCSS, mg/Kg) <br />RPD Relatve Percent Difference, calwlatlon used for Duplicate OC Types <br />Upper Upper Recovery Limit, in % (except for LCSS, mglKg) <br />Sample Value of the Sample of interest <br />ga``~`5v,%,J.;?..y. e.`~~'~'a~_M;~t-*cTS~i+~.w:¢~ -^~..s~.f--~.: s~'~k~~.G..r~'-NS'Rk`~_z_. 3~.znuxnm` `-'_,_ sv~'~~.°~'_.a~~i."F~~,'~`.a_~--`Li~f~*¢;v"c'~:3c~; ?3"srt <br />~ AS Analytical Spike (Post Digestion) LFM Laboratory Fortified MaWx <br />ASD Analytical Spike (Post Digestion) Duplicate LFMD Laboratory Fortified Matrix Duplicate <br />DUP Sample Duplicate LRB Laboratory Reagent Blank <br />LCSS Laboratory Control Sample -Soil MS/MSD Matrix Spike/Matdz Spike Duplio[e <br />LCSW Laboratory Contml Sample -Water PBS Prep Blank -Soil <br />LFB Laboratory Fortified Blank PBW ro Prep Blank -Water <br />~':=-ric~'u-"iv se-r xaa.s..a. 'v" yr1...Y, t.'g:e3y -tt~, .~,rf ']['~;.`rr~a'4 e+~~iai'vr e2GkS~ ~ a r a v.~e~MA`v-~iY ~~~x .4~r e~ <br />• )~aa-~.~ ~.r--.'-.tG. ._:.~;x cs.e,~ T a, __u_._..s ~.s~-~._.-~~.ms~z. 'r/~.:.._.Ea~~Y~"[ <br />Blanks Vedfies that there is rw or rtunimal contaminafion in the prep method procedure <br />Conhol Samples Verifies the accuracy of the method, including the prep procedure. <br />Duplicates Verdes the precision of the instmment and/or method. <br />SpikeslFortified Mahix Determines sample matrix interferences, if any. <br />~a gaf~"FI:t > F"cn.t! ~*'!~ s~~iili-'~~'y'r~'ry"? ~.,. 4^.. ~R '~'~ ..& '"^' w..rn t•-.`~'~ z' -a-++~r~...~~'"i <br />.°i._L.t[.__. _! ,~t~~zc~..,..;,:?.~5.-~...~:~~._~r~- ,.i .;.«~,~4: ~'~'P'~4tCn3r~ .ru'. >'.l_~ .,aa~ ~~_.~n-.r... .._ i.z> <br />B Analyte concentration detected at a value between MDL and PDL d <br />R Poor spike recovery accepted beceuse the other spike in the set fell within the given limits. <br />T High Relative Percent Difference (RPD) accepted because sample concentrafions are less than 10x the MDL. <br />U Analyte was analyzed for but not detected at the indicated MDL <br />V High blank data accepted because sample concentration is 10 times higher than blank concentration <br />W Poor recovery for Silver quality control is accepted because Silver often precipitates with Chloride. <br />X Quality control sample is out of centrd. <br />Z Poor spike recovery is accepted because sample cencenhation is four times greater than spike concentration. <br />~.. err °.:.v --. ,-:. ~ --_.~ a -i. ~ - ~.,-_ <br />I .r <br />(1) EPA 600/4-83-020. Methods for Chemical Analysis of Water and Wastes. March 1983. <br />(2) EPA 600/R-93-100. Methods for the Determination of Inorganic Substances in Environmental Samples, August 1993. <br />(3) EPA 600/R-94-711. Methods for the Determination of Metals in Environmental Samples -Supplement I, May 1094. <br />(5) EPA SW-846. Test Methods for Evaluating Solid Waste, Third Edition with Update II, September 1994. <br />(6) Standard Methods for the F~amination of Water and Wastewater, 19th edition, 1995. <br />y,~ ' x:a Yeir - '+-,~*'~..€'" ~.'s~2 ~~,. . ,s ^~ ~ ~-~,-..,~~`° .,.. P wrr i u, ,Y ~ p r's.i.• t y-t, <br />1 __~_y ~Effi~ .Iew~, ,-'4 si,_-~_•.?~?..~_.Y...._.; '~z >. .- ._2_2~,.~. -no_..::.~"~.'::__.s_v..,'~'~l'~_.7'M.~.:i. ?,~'=. <br />(1) QC results calculated from raw data. Results may vary slightly if the rounded values are used in the calculations. <br />• (2) Soil, Sludge, and Plant matrices (or Inorganic analyses are reported on a dry weigh) basis. <br />(3) Animal matrices for Inorganic analyses are reported on an "as received" basis. <br />REPIN03.71.00.07 <br />L33193: Page ? of 9 <br />