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AUZ Laboratories, Inc. • - - • - • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 @ - • • <br /> Ensero Solutions ACZ Project ID: L74959 <br /> METHOD,ACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br /> L74959-01 VVG548075 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG549132 Fluoride SM450OF-C MA Recovery for either the spike or spike duplicate was outside <br /> of the acceptance limits;the RPD was within the <br /> acceptance limits. <br /> WG548826 Nitrate/Nitnte as N M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG548459 Phosphorus,total W65 1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG548028 Residue,Filterable(TDS)@180C SW540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG548085 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> SM2540D Z3 Sample volume yielded a residue less than 2 5 mg <br /> WG548221 Sulfate D516-02/-07/-11- M3 The spike recovery value is unusable since the analyte <br /> TURBIDIMETRIC concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> D516-02/-07/-11- RA Relative Percent Difference(RPD)was not used for data <br /> TURBIDIMETRIC validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG549397 Total Hot Plate Digestion M200 2 ICP-MS DJ Sample dilution required due to insufficient sample. <br /> REPAD.15.06.05.01 <br /> L74959-2210141458 Page 11 of 20 <br />