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1�zkofi '• Pace Analytical <br /> 1673 Terra Avenue Sheridan,WY 82801 ph:(307)672-8945 <br /> ANALYTICAL QC SUMMARY REPORT <br /> CLIENT: Grand Island Resources Date: 8/17/2022 <br /> Work Order: S2207411 Report ID: S2207411001 <br /> Project: Waste Rods Characterization <br /> BLM Sulfur Forms Sample Type LCS Units: % <br /> LCS(08/17/22 11:41) RunNo:202963 <br /> Analyte Result RL Spike Ref Samp %REC %Rec Limits Qual <br /> Hot Water Sulfur-LECO 0.26 0.01 0.33 79.7 43.4-102 <br /> HCL Sulfur-LECO 0.19 0.01 0.23 82.7 37.1-108 <br /> HNO3 Sulfur-LECO 0.03 0.01 0.03 93.9 <br /> pH-Soil Sample Type LCS Units: s.u_ <br /> CONTROL(08/09/22 08:50) RunNo:202700 <br /> Analyte Result RL Spike Ref Samp %REC %Rec Limits Qual <br /> pH 7.1 0.1 7.1 100 96-104 <br /> Sulfur Forms Sample Type LCS Units: % <br /> LCS(08/01/22 16:53) RunNo:202468 <br /> Analyte Result RL Spike Ref Samp %REC %Rec Limits Qual <br /> Total Sulfur 0.68 0.01 0.67 101 72-121 <br /> Page 1 of 1 <br />