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ACZ Laboratories, Inc. • <br /> 2773 Downhill Drive Steamboat Springs,CO 80487 (800)334-5493 $ • • <br /> Ensero Solutions ACZ Project ID: L73416 <br /> L73416-01 NG543878 Arsenic,total M200 8 ICP-MS VC CCV recovery was above the acceptance limits.Target <br /> analyte was not detected in the sample[<MDL]. <br /> WG543476 Cyanide,WAD SM4500-CN I,E-Colodmetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> W G544045 Nitrate/Nftnte as N M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> W G544069 Phosphorus,total M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG543098 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG543616 Sulfate D516-02/-07/-11- M3 The spike recovery value is unusable since the analyte <br /> TURBIDIMETRIC concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> L73416-02 NG543476 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG544045 Nitrate/Nitnte as N M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> W G544069 Phosphorus,total M365 1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG543098 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> W G543616 Sulfate D516-02/-07/-11- M3 The spike recovery value is unusable since the analyte <br /> TURBIDIMETRIC concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable <br /> WG543936 Total Recoverable Digestion M200.2 ICP-MS DJ Sample dilution required due tolnsufficient sample <br /> REPAD 15.06.05.01 <br /> L73416-2206301248 Page 13 of 23 <br />