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ADZ Laboratories, Inc. • • • - • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • <br /> Ensero Solutions ACZ Project ID: L72339 <br /> METHODACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br /> L72339.01 NG540767 Antimony,total recoverable M200.8 ICP-MS LA Recovery for target analyte in the control sample(LCS or <br /> LFB)exceeded the acceptance criteria. Target analyte was <br /> not detected in the sample[<MDL]. <br /> WG539842 Cyanide,WAD SM4500-CN I,E-Colodmetric w/ Q6 Sample was received above recommended temperature <br /> distillation <br /> SM4500-CN I,E-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG540645 Fluoride SM450OF-C Q6 Sample was received above recommended temperature. <br /> WG540746 Molybdenum,dissolved M200 7 ICP VC CCV recovery was above the acceptance limits Target <br /> analyte was not detected in the sample[<MDL] <br /> WG540857 Nitrate/Nitrite as N M353 2-H2SO4 preserved Q6 Sample was received above recommended temperature. <br /> M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<lox MDL) <br /> WG539918 Phosphorus,total M365.1-Auto Ascorbic Acid M2 Matrix spike recovery was low,the recovery of the <br /> (digest) associated control sample(LCS or LFB)was acceptable <br /> M365.1-Auto Ascorbic Acid Q6 Sample was received above recommended temperature. <br /> (digest) <br /> M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG539704 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature. <br /> WG539797 Residue,Non-Filterable(TSS)@105C SM2540D Q6 Sample was received above recommended temperature. <br /> SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG540541 Sulfate D516-02/-07/-11- 06 Sample was received above recommended temperature. <br /> TURBIDIMETRIC <br /> L72339-02 NG540767 Antimony,total recoverable M200.8 ICP-MS LA Recovery for target analyte in the control sample(LCS or <br /> LFB)exceeded the acceptance crtena. Target analyte was <br /> not detected in the sample[<MDL] <br /> WG539842 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ Q6 Sample was received above recommended temperature <br /> distillation <br /> SM4500-CN I,E-Colonmetnc w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG540645 Fluoride SM450OF-C Q6 Sample was received above recommended temperature. <br /> WG540746 Molybdenum,dissolved M200 7 ICP VC CCV recovery was above the acceptance limits Target <br /> analyte was not detected in the sample[<MDL] <br /> WG540857 Nitrate/Nitrite as N M353.2-H2SO4 preserved Q6 Sample was received above recommended temperature <br /> M353 2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG539918 Phosphorus,total M365 1-Auto Ascorbic Acid M2 Matrix spike recovery was low,the recovery of the <br /> (digest) associated control sample(LCS or LFB)was acceptable. <br /> M365.1-Auto Ascorbic Acid Q6 Sample was received above recommended temperature <br /> (digest) <br /> M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG539704 Residue,Filterable(TDS)@180C SM2540C Q6 Sample was received above recommended temperature <br /> WG539797 Residue,Non-Filterable(TSS)@105C SM2540D Q6 Sample was received above recommended temperature. <br /> SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> SM2540D Z3 Sample volume yielded a residue less than 2 5 mg <br /> WG540541 Sulfate D516-02/-07/-1 l- Q6 Sample was received above recommended temperature. <br /> TURBIDIMETRIC <br /> REPAD.15.06.05.01 <br /> L72339-2205261013 Page 12 of 22 <br />