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Physicochemical Analysis and Methods <br />• pH, sat paste <br />• Conductivity @ 25 C <br />• Saturation <br />• Texture <br />• Ca (sat paste) <br />• Mg (sat paste) <br />• Na (sat paste) <br />• SAR <br />• Cation Exchange Capacity <br />• Exchangeable Na <br />• Exchangeable Sodium % <br />• Se (hot water) <br />• B (hot water) <br />• NO3 as N (water) <br />• Mo (NH4 oxalate) <br />• As, Hg, Pb, Zn, Fe, and Mn <br />(AB -DTPA Extractable) <br />• NP as CaCO3 <br />• Sulfur Forms in % <br />• Acid Generation Potential (AGP), <br />Acid Neutralization Potential (ANP) <br />and Acid Base Potential (ABP) <br />• AGP:ANP <br />Sample Preparation Methods <br />• Air Dry @ 34'C <br />• NH4 oxalate <br />• Crush and Pulverize <br />• AB -DTPA extraction <br />• Hot water extraction <br />• Saturated Paste Extraction <br />• Water extraction <br />RULE 2 PERMITS <br />USDA No.60 (21A) <br />EPA Method M 120. 1 -meter,w/sat paste <br />USDA No. 60 (2) <br />ASTM D 422 Hydrometer <br />EPA Method M6010 ICP <br />EPA Method M6010 ICP <br />EPA Method M6010 ICP <br />calculation <br />NH4Oac, USDA No. 60 (19) <br />NH4Oac extractable, M6010B ICP <br />Exchangeable Na/CEC <br />SM3500-Se.0 <br />EPA Method M6010 ICP <br />EPA Method M353.2 -automated <br />EPA Method M6010 ICP <br />EPA Method M6010 ICP <br />EPA Method M600/2-78-054 3.2.3 <br />EPA Method M600/2-78-054 3.2.4 <br />EPA Method M600/2-78-054 1.3 <br />calculation <br />USDA No. 1, 1972 <br />ASA No. 9, Part 2 1965 M 74.2 <br />USDA No. 1, 1972 <br />ASA No. 9, Part 2, 1982 M3-5.2 <br />ASA No. 9, Part 2 1965 M 80-3 <br />USDA Handbook 66, M@ <br />ASA No.9 M10-2.3.2 <br />Exploration Test Boring Results Summary <br />The physicochemical data from overburden sampling by Colowyo and Consol are provided in Exhibit 6, <br />Item 6. The analytical data from Consol includes: pH, conductivity, saturation percentage, percent sand, <br />silt, and clay, calcium, magnesium, sodium, sodium absorption ratio, boron, molybdenum, selenium, <br />nitrate -nitrogen, arsenic, mercury, lead, zinc, iron, and manganese (AB -DTPA Extractable), acid - <br />generating potential, sulfur forms, and total sulfur. The acid -generating potential (AGP) for these <br />samples was calculated based on pyritic -sulfur percent. <br />South Taylor/Lower Wilson — Rule 2, Page 16 Revision Date: 11/18/16 <br />Revision No.: MR -163 <br />