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ADZ Laboratories, Inc. • • - • - • <br /> 2773 Downhill Drive Steamboat Sprigs,CO 80487 (800)334-5493 - • • <br /> Ensero Solutions ACZ Project ID: L70424 <br /> METHODACZ ID WORKNUM PARAMETER QUAL DESCRIPTION <br /> L70424-01 NG534480 Antimony,total recoverable M200 8 ICP-MS M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG533955 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG534197 NRrate/NRnte as N M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG534316 Phosphorus,total M365 1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG533540 Residue,Non-FiRerable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<lox MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2 5 mg <br /> WG534737 Uranium,total M200 8 ICP-MS M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level The recovery of the associated control sample(LCS <br /> or LFB)was acceptable <br /> L70424-02 NG534480 Antimony,total recoverable M200.8 ICP-MS M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG533955 Cyanide,WAD SM4500-CN I,E-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG534197 Nitrate/Nitrite as N M353.2-H2SO4 preserved RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL) <br /> WG534316 Phosphorus,total M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL) <br /> WG533540 Residue,Non-FiRerable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2 5 mg <br /> WG534737 Uranium,total M200 8 ICP-MS M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> REPAD.15.06.05.01 <br /> L70424-2201310853 Page 13 of 23 <br />