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ACZ <br /> Laboratories, Inc. ro -0. <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 &' ' <br /> u; tiv <br /> Ouray Silver Mines ACZ Project ID: L66632 <br /> vrr . 'U" <br /> L66632-01 NG521725 Calcium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG522956 Chloride SM4500CI-E RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG522398 Cyanide,total M335.4-Colorimetric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG521725 Manganese,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG522199 Phosphorus,total M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG521865 Residue,Filterable(TDS)@180C SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG521805 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG521725 Sodium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG523091 Sulfate D516-021-07/-11- M2 Matrix spike recovery was low,the recovery of the <br /> TURBIDIMETRIC associated control sample(LCS or LFB)was acceptable. <br /> D516-02/-07/-11- RA Relative Percent Difference(RPD)was not used for data <br /> TURBIDIMETRIC validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> L66632-02 NG521725 Calcium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG522956 Chloride SM4500CI-E RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG522398 Cyanide,total M335.4-Colon metric w/ RA Relative Percent Difference(RPD)was not used for data <br /> distillation validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG521725 Manganese,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG522199 Phosphorus,total M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> WG521865 Residue,Filterable(TDS)@180C SM2540C RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG521805 Residue,Non-Filterable(TSS)@105C SM2540D RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> SM2540D Z3 Sample volume yielded a residue less than 2.5 mg <br /> WG521725 Sodium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG523091 Sulfate D516-02/-07/-11- M2 Matrix spike recovery was low,the recovery of the <br /> TURBIDIMETRIC associated control sample(LCS or LFB)was acceptable. <br /> D516-02/-07/-11- RA Relative Percent Difference(RPD)was not used for data <br /> TURBIDIMETRIC validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1 Ox MDL). <br /> REPAD.15.06.05.01 <br /> L66632-2107141355 Page 29 of 36 <br />