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AAL <br /> 2103123 <br /> Metals: <br /> The samples were analyzed following SW-846, 3rd Edition procedures. Analysis by ICPMS followed <br /> method 6020B and the current revision of SOP 827. Mercury analysis by CVAA followed method <br /> 7470A and the current revision of SOP 812. <br /> The samples for dissolved metals had been filtered prior to receipt. <br /> Matrix spike recoveries could not be evaluated for the following analyte: <br /> Anal)de Sample ID <br /> Calcium 2103123-3 <br /> The concentration of this analyte in the native sample was greater than four times the concentration <br /> of matrix spike added during the digestion. When sample concentration is that much greater than the <br /> spike added, spike recoveries may not be accurate. The laboratory control sample indicates that the <br /> digestion and analysis were in control. <br /> All acceptance criteria were met. <br /> Inorganics: <br /> The samples were analyzed following SW-846, EMSL and Standard Method procedures for the <br /> current revisions of the following SOPs and methods.- <br /> Analyte Method SOP# <br /> Alkalinity SM2320B 1106 <br /> Bicarbonate SM2320B 1106 <br /> Carbonate SM2320B 1106 <br /> Total ryanirle 9014 1110 <br /> Nitrate/nitrite as N 353.2 Revision 2.0 1127 <br /> pH SM4500-H+ B 1126 <br /> TDS SM2540C 1101 <br /> Chloride 300.0 Revision 2.1 1113 <br /> Fluoride 300.0 Revision 2.1 1113 <br /> Nitrate as N 300.0 Revision 2.1 1113 <br /> Nitrite as N 300.0 Revision 2.1 1113 <br /> Sulfate 300.0 Revision 2.1 1113 <br /> All acceptance criteria were met. <br /> ADDRESS 225 Commerce Drive,Fort Collins Colorado 80524 USA PHONE+1 970 490 1 511 FAX+1 970 490 1 522 3 of 31 <br /> ALS GROUP USA,CORP Part of the ALS Group An ALS limited Company <br />