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Laboratories, Inc. - - • - • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 - • • ' <br /> Golder Associates ACZ Project ID: L62895 <br /> METHODACZ ID WVORKNUM PARAMETER QUAL DESCRIPTION ' <br /> L62895-01 WG509956 Beryllium,dissolved M200.8 ICP-MS IA Internal standard recovery exceeded the acceptance limits. <br /> Concentration of associated target analyte(s)in the ' <br /> sample is<MDL. <br /> WG510206 Chloride M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<10x MDL). <br /> WG510118 Chromium,dissolved M200.8 ICP-MS DD Sample required dilution due to matrix color or odor. ' <br /> Copper,dissolved M200.8 ICP-MS DD Sample required dilution due to matrix color or odor. <br /> WG509814 Cyanide,Free D6888-09/OIA-1677-09 DE Sample required dilution. See Case Narrative. <br /> WG509974 Fluoride SM450OF-C DD Sample required dilution due to matrix color or odor. ' <br /> SM450OF-C MA Recovery for either the spike or spike duplicate was <br /> outside of the acceptance limits;the RPD was within the <br /> acceptance limits. <br /> WG510118 Lead,dissolved M200.8 ICP-MS DD Sample required dilution due to matrix color or odor. <br /> WG510086 Mercury,dissolved M245.1 CVAA MA Recovery for either the spike or spike duplicate was ' <br /> outside of the acceptance limits;the RPD was within the <br /> acceptance limits. <br /> WG510068 Nitrate/Nitrite as N,dissolved M353.2-Automated Cadmium HE Analysis performed past holding time. Method holding <br /> Reduction time is less than or equal to 7 days and sample was , <br /> received with less than half of the holding time remaining <br /> (refer to item C5 of ACZ's Terms 8 Conditions). <br /> W G509809 Nitrite as N,dissolved M353.2-Automated Cadmium RA Relative Percent Difference(RPD)was not used for data <br /> Reduction validation because the concentration of the duplicated ' <br /> sample is too low for accurate evaluation(<10x MDL). <br /> W G510050 pH SM4500H+B ZW Method deviation. The sample was centrifuged prior to <br /> analysis due to high solid content. <br /> W G510226 Silver,dissolved M200.8 ICP-MS D1 Sample required dilution due to matrix. <br /> M200.8 ICP-MS DD Sample required dilution due to matrix color or odor. ' <br /> WG510206 Sulfate M300.0-Ion Chromatography RA Relative Percent Difference(RPD)was not used for data <br /> validation because the concentration of the duplicated <br /> sample is too low for accurate evaluation(<1Ox MDL). <br /> W G510050 Total Alkalinity SM2320B-Titration ZW Method deviation. The sample was centrifuged prior to ' <br /> analysis due to high solid content. <br /> W G510118 Uranium,dissolved M200.8 ICP-MS DD Sample required dilution due to matrix color or odor. <br /> REPAD.15.06.05.01 <br /> L62895-2012041237 Page 14 of 22 <br />