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element concentrations present in solid samples and/or to bring over range target analyte <br /> concentrations into the linear calibration range of the instrument. Samples 344616001 (Sunday <br /> MW 1) and 344616002 (Sunday MW 1D)-ICP were diluted because silver was suppressed and <br /> the sodium concentration exceeded the linear calibration range of the instrument. <br /> Preparation Information <br /> The samples in this SDG were prepared exactly according to the cited SOP. <br /> Miscellaneous Information <br /> Electronic Packaging Comment <br /> This data package was generated using an electronic data processing program referred to as <br /> virtual packaging. In an effort to increase quality and efficiency, the laboratory has developed <br /> systems to generate all data packages electronically. The following change from traditional <br /> packages should be noted: <br /> Analyst/peer reviewer initials and dates are not present on the electronic data files. Presently, all <br /> initials and dates are present on the original raw data. These hard copies are temporarily stored in <br /> the laboratory. An electronic signature page inserted after the case narrative will include the data <br /> validator's signature and title. The signature page also includes the data qualifiers used in the <br /> fractional package. Data that are not generated electronically, such as hand written pages, will be <br /> scanned and inserted into the electronic package. <br /> Data Exception (DER) Documentation <br /> Data exception reports (DERs) are generated to document procedural anomalies that may deviate <br /> from referenced SOP or contractual documents. A data exception report was not required for this <br /> SDG. <br /> Additional Comments <br /> Additional comments were not required for this SDG. <br /> Certification Statement <br /> Where the analytical method has been performed under NELAP certification, the analysis has <br /> met all of the requirements of the NELAC standard unless otherwise noted in the analytical case <br /> narrative. <br /> Review Validation: <br /> GEL requires all analytical data to be verified by a qualified data validator. In addition, all data <br /> designated for CLP or CLP-like packaging will receive a third level validation upon completion <br /> of the data package. <br /> The following data validator verified the information presented in this case narrative: <br /> Reviewer Date: <br /> D 0 <br /> Page 21 of 94 <br />