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GEL Laboratories LLC DER Report No.: 1233058 <br /> Form GEL-DER <br /> Revision No.: <br /> DATA EXCEPTION REPORT <br /> Mo.Day Yr. Division: Quality Criteria: Type: <br /> 17-OCT-13 Industrial Specifications Process <br /> Instrument Type: Test/Method: Matrix Type: Client Code: <br /> ICP/MS EPA 200.8 Drinking Water CTLA, DNMI, LANC,TOXC <br /> Batch ID: Sample Numbers: <br /> 1335815 See Below <br /> Potentially affected work order(s)(SDG):333974,333975,333976,333977,333978,333979,334016,334021,334023,334024,334116,334119,334166,334 <br /> Application Issues: 167,334261,334262 <br /> Failed Recovery for MS/PS <br /> Specification and Requirements DER Disposition: <br /> Exception Description: <br /> 1. Failed Recovery for MS/PS: The matrix spike(1202959472,1202965771)recovery failed outside of the <br /> control limits for TI and U due to possible matrix interferences and/or non- <br /> QC 1202959472MS,1202965771 MS homogeneity. Per GEL's accredited methods and SOPS,a corrective <br /> action is not required and the data is qualified and reported. <br /> Originator's Name: Data Validator/Group Leader: <br /> Samantha Jacobs 17-OCT-13 Paul Boyd 17-OCT-13 <br /> Page 40 of 99 <br />