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AL <br /> Laboratories, Inc. <br /> • • • • <br /> 2773 Downhill Drive Steamboat Springs, CO 80487 (800)334-5493 0 - • • <br /> Western Water and Land Inc. ACZ Project ID: L20770 <br /> METHOD QUAL DESCRIPTION <br /> L20770-01 WG372031 Sodium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG371930 Nitrate/Nitrite as N,dissolved M353.2-Automated Cadmium H3 Sample was received and analyzed past holding time. <br /> Reduction <br /> M353.2-Automated Cadmium RA Relative Percent Difference(RPD)was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> Nitrite as N,dissolved M353.2-Automated Cadmium H3 Sample was received and analyzed past holding time. <br /> Reduction <br /> M353.2-Automated Cadmium RA Relative Percent Difference(RPD)was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> WG372655 Phosphorus,total M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> L20770-02 WG372031 Sodium,dissolved M200.7 ICP M3 The spike recovery value is unusable since the analyte <br /> concentration in the sample is disproportionate to the spike <br /> level.The recovery of the associated control sample(LCS <br /> or LFB)was acceptable. <br /> WG371930 Nitrate/Nitrite as N,dissolved M353.2-Automated Cadmium HE Analysis performed past holding time. Method holding time <br /> Reduction is less than or equal to 7 days and sample was received <br /> with less than half of the holding time remaining(refer to <br /> item C5 of ACZ's Terms&Conditions). <br /> M353.2-Automated Cadmium RA Relative Percent Difference(RPD)was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> Nitrite as N,dissolved M353.2-Automated Cadmium HE Analysis performed past holding time. Method holding time <br /> Reduction is less than or equal to 7 days and sample was received <br /> with less than half of the holding time remaining(refer to <br /> item C5 of ACZ's Terms&Conditions). <br /> M353.2-Automated Cadmium RA Relative Percent Difference(RPD)was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> WG372655 Phosphorus,total M365.1-Auto Ascorbic Acid RA Relative Percent Difference(RPD)was not used for data <br /> (digest) validation because the sample concentration is too low for <br /> accurate evaluation(<10x MDL). <br /> WG372145 Total Alkalinity SM2320B-Titration ZW Method deviation. The sample was centrifuged prior to <br /> analysis due to high solid content. <br /> R E PA D.15.06.05.01 <br /> L20770-1410281323 Page 15 of 26 <br />